运用TSQ Quantum Access MAX分析饮用水中均三氮苯类除草剂
简介
Thermo Scientific TraceFinder software includes built-in workflows for streamlining routine analyses in environmental and food safety laboratories. By incorporating a database of liquid chromatography-mass spectrometry (LC/MS) methods that can be customized to include unique compounds, TraceFinder™ allows the analyst to access commonly encountered contaminants found in the environment. To demonstrate the capabilities of this software, a mixture of triazine compounds spiked into drinking water samples was analyzed. Using direct injections of 20 mL samples (with on-line preconcentration), low- and sub-pg/mL (ppt) levels were detected. The ability to analyze these drinking water samples with on-line preconcentration saves considerable time and expense compared to solid phase extraction techniques.
目标
To demonstrate the ease-of-use of TraceFinder software for the analysis of triazine herbicides in water samples.
实验仪器
TSQ Quantum Access MAX triple stage quadrupole mass spectrometer
结论
In this application note, TraceFinder software was used in conjunction with an online preconcentration system, Equan™, for the robust and reproducible analysis of large volumes of drinking water. Triazines were quantitated at the sub-ppt level, and several commercial bottled drinking water samples and one sugar-free soda sample were analyzed for the presence of triazines. Only one sample contained any traces of triazines: a commercial drinking water sample tested positive for atrazine. TraceFinder can also be used for traditional LC/MS applications, minimizing method development time. The method development capabilities and Compound Datastore of TraceFinder allowed for the quick creation of a method for the analysis of these compounds.
