Dionex Integrion(IN) HPIC 高压离子色谱系统

Pump泵

类型Type：Dual-piston (in series), microprocessor controlled, constant 10 mm primary stroke length, variable speed Isokinetic with Eluent Precompression

组成Construction： Chemically inert, metal-free PEEK pump heads and flow path; compatible with aqueous eluents from pH 0–14 and reversed-phase solvents such as methanol and acetonitrile

Pressure Range 0–41 MPa (0–6000 psi)

Flow Rate Range 0.000–10.000 mL/min with ability to set flow increments at 0.001 mL/min

Flow Rate Precision < ±0.1%

Flow Rate Accuracy < ±0.1%

Pressure Ripple < 1% at 1.0 mL/min, typical

Vacuum Degasser Integrated, optional

Piston Seal Wash Optional, automatic operation

Eluent On/Off Valve Electrically actuated, standard

Leak Sensor Optical, standard

淋洗液发生器Eluent Generator

Eluent Types Up to two eluent generator cartridges

KOH, LiOH, NaOH; Carbonate; Carbonate/Bicarbonate; MSA

Eluent Concentration Range 0.1–100 mM

Flow Rates 0.1–3 mL/min

1.0 mL/min eluent concentration is limited

Maximum Operating Pressure Dionex EGC 500 cartridge: 35 MPa (5000 psi)

Maximum Solvent Concentration Cations: 0%

Anions (hydroxide): 25% methanol (KOH, NaOH and LiOH cartridges);

Anions (carbonate/bicarbonate): None

Gradient Profiles Standard - any combination of linear, convex and concave positive and negative gradient profiles

柱温箱Column Compartment

Injection Valves Up to two high-pressure valves, either 6- or 10-port

Columns Supported Up to two 1-9 mm i.d., maximum length 250 mm analytical column with

50 mm guard column

Constant Temperature Zone Optional

Temp. Range: 30 to 80 °C (86 to 176 °F); minimum 5 °C above ambient

Temperature Accuracy: ±0.5 °C at 30 °C)

Temperature Stability: ±0.2 °C (at 30 °C)

Time to Equilibration (ambient to ambient plus 20 °C): 20 minutes

检测器Detector Compartment

Constant Temperature Zone Optional

Temp. Range: 15 (or 20 °C below ambient) to 40 °C (59 to 104 °F)

Temperature Accuracy: ±0.5 °C (at 15 °C)

Temperature Stability: ±0.2 °C (at 15 °C)

Time to Equilibration (ambient to ambient minus 20°C): 30 minutes

抑制模式Suppression Modes

Chemical Suppression： 2 mm and 4 mm, anion and cation, membrane suppression

Electrolytic Suppression Recycle Mode： 2 mm and 4 mm, anion and cation, membrane suppression

Electrolytic Suppression External Water Mode：2 mm and 4 mm, anion and cation, membrane suppression

Non-Suppressed Conductivity： Supported - both anion and cation

电导检测器Conductivity Detector

Electronics Type Microprocessor controlled digital signal processing, autoranging

Cell Drive 8 kHz square wave

Linearity 1%

Resolution 0.00238 nS/cm

Output Range Digital Signal Range: 0–15,000 µS/cm

Analog Signal Range: 0–15,000 µS/cm

Noise, Wet ≤ 0.2 nS at 23 µS/cm background

≤ 0.1 nS at 1 µS/cm background

Filter Rise times 0 to 10 s, programmable

Sampling Rate 1 to 100 Hz, user settable or automatic

Cell Temperature 7 °C above ambient to 60 °C maximum

Cell Temperature Stability < 0.001 °C

Cell Temperature Compensation Default 1.7% per °C; programmable from 0–3% per °C

Flow Cell Maximum Pressure 10 MPa (1500 psi)

Flow Cell Volume 0.7 µL

Cell Electrodes Passivated 316 stainless steel. Compatible with MSA

Cell Body Chemically inert polymeric material

Heat Exchanger Inert, tortuous-path for low longitudinal dispersion

电化学检测器Electrochemical Detector

Electronics Type Microprocessor controlled digital signal processing

Electronic Noise, Wet IPAD (Au electrode) < 50 pC at 10 mM KOH, DC Amperometry (GC) < 10 pA

Potential Range -2.0 to 2.0 V in 0.001 V increments

Signal range (Digital and Analog) Integrated Amperometry: 50 pC to 200 µC DC Amperometry: 5 pA to 74 µA

Filter 0–10 s response time, user settable

Control Mode Local or remote control using relay closures or TTL, or control using Chromeleon CDS software via

DC module

Cell Body Titanium body. Compatible with 2–7 mm i.d. columns

Working Electrodes Conventional: gold, glassy carbon, platinum, and silver

Disposable: gold, platinum, carbon, and silver

Reference Electrode pH-Ag/AgCl combination, one piece design

PdH, one piece design

Autoranging Yes

Analog Output User selectable full scale of 10, 100, or 1000 mV

Cell Volume at Working Electrode < 0.2 µL

Maximum Cell Operating Pressure 0.7 MPa (100 psi)

供电Internal Power Supplies

Internal Power supplies Constant current (CC) or constant voltage (CV) power supplies

Option 1: 1 channel CC [0 - 500 mA] or CV [0 – 36 V]

Option 2: 2 channels CC [0 - 500 mA] or CV [0 – 36 V]

Option 3: 1 channel CC [0 - 500 mA] & 2 channels CC [0 - 500 mA] or CV [0 – 36 V]

Option 4: 1 channel CC [0 - 500 mA] & 4 channels CC [0 - 500 mA] or CV [0 – 36 V]

Product 

系统软件System Software

Software Chromeleon CDS software, version 7.2 or higher

Automated Workflow Wizards Standard feature

System Smart Startup and Shutdown Standard feature

Automation Support of 3rd Fully controls over 400 different instruments from more than 30 manufacturers, including GC, HPLC,

Party Instruments and MS

Customizable System Control Panels Standard feature

Signal Channels Detector signals and pump pressure as standard

Data Trending Plots All numerical device parameters

System Status Virtual Channels Standard feature

Network Failure Protection Standard feature for networked installations

System Trigger Commands and Conditionals：Standard feature

Daily Audit Trail Standard feature

Sample Audit Trail Standard feature

System Calibration Storage Factory, present and previous. Completely user selectable.

Customized Reporting Standard feature with unlimited report sheets

GLP Compliance Optional

物理性能Physical Specifications

Power Requirements 100–240 V ac, 50-60 Hz autoranging

Operating Temperature 4–40 °C (40–104 °F); cold-room compatible (4 °C) as long as system power remains on

Operating Humidity Range 5–95% relative, noncondensing

Control Modes Full control through front panel and Chromeleon CDS software; alternative control through TTL or relay

closures; two relay outputs, two TTL outputs, four programmable inputs

USB Communication Protocol One USB input; one built-in two-output USB hub

Leak Detection Built-in, optical sensor

Dimensions (h × w × d) 62.5 × 30.0 × 55.9 cm

(24.6 × 11.8 × 22 inches)

Weight 41 kg (90 lb)

赛默飞新推出的Dionex Integrion高压离子色谱系统非常直观、简洁易用，并具有应对挑战性实验室工作流程的能力。这也是自从赛默飞从2011年收购戴安公司以来的推出的第一款新的离子色谱系统。

该HPIC系统采用了以前只在高端系统中才使用的功能，包括高压和选择性的电化学检测器。拥有简单、合理的流路设计和集成性能的功能，包括全系统智能监控，并在稳定可靠的情况下提供更快的运行速度。

具有以下功能：

1、易于安装的IC PEEK Viperpei配件，使操作简单，减少峰扩散和谱带增宽，提高色谱分辨率。

2、本地语言支持的平板电脑，即使远离仪器也能灵活地与IC控制器相连。

3、 通过消耗品设备监控记录追踪系统和消耗品性能，调试安装错误，将数据存储于安全的云服务器上，提高预防性维修和zei大运行时间。

4、热稳压器舱延长消耗品的寿命。

5、赛默飞变色龙数据软件系统（CDS）简化工作流程，从而大大节省了从样本到结果的时间。

6、 自动生成洗脱液。