17.180.30 光学测量仪器 标准查询与下载



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1.1 This practice covers requirements for the validation of measurements made by laboratory, field, or process (online or at-line) infrared (nearor mid-infrared analyzers, or both), and Raman analyzers, used in the calculation of physical, chemical, or quality parameters (that is, properties) of liquid petroleum products and fuels. The properties are calculated from spectroscopic data using multivariate modeling methods. The requirements include verification of adequate instrument performance, verification of the applicability of the calibration model to the spectrum of the sample under test, and verification that the uncertainties associated with the degree of agreement between *A Summary of Changes section appears at the end of this standard Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. 1 the results calculated from the infrared or Raman measurements and the results produced by the PTM used for the development of the calibration model meets user-specified requirements. Initially, a limited number of validation samples representative of current production are used to do a local validation. When there is an adequate number of validation samples with sufficient variation in both property level and sample composition to span the model calibration space, the statistical methodology of Practice D6708 can be used to provide general validation of this equivalence over the complete operating range of the analyzer. For cases where adequate property and composition variation is not achieved, local validation shall continue to be used. 1.1.1 For some applications, the analyzer and PTM are applied to the same material. The application of the multivariate model to the analyzer output (spectrum) directly produces a PPTMR for the same material for which the spectrum was measured. The PPTMRs are compared to the PTMRs measured on the same materials to determine the degree of agreement. 1.1.2 For other applications, the material measured by the analyzer system is subjected to a consistent additive treatment prior to being analyzed by the PTM. The application of the multivariate model to the analyzer output (spectrum) produces a PPTMR for the treated material. The PPTMRs based on the analyzer outputs are compared to the PTMRs measured on the treated materials to determine the degree of agreement. 1.1.3 In some cases, a two-step procedure is employed. In the first step, the analyzer and PTM are applied to the measurement of a blendstock material. In a second step, the PPTMRs produced in Step 1 are used as inputs to a second model that predicts the results obtained when the PTM is applied to the analysis of the finished blended product produced by additivation to the blendstock. If the analyzer used in the first step is a multivariate spectroscopic based analyzer, then this practice is used to access the degree of agreement between PPTMRs and PTMRs. Otherwise, Practice D3764 is used to compare the PPTMRs to the PTMRs for this blendstock to determine the degree of agreement. Since this second step does not use spectroscopic data, the validation of the second step is done using Practice D3764. If the first step uses a multivariate spectrophotometric analyzer, then only samples for which the spectra are not outliers relative to the multivariate model are used in the second step. Note that the second model might accommodate variable levels of additive material addition to the blend stock. 1.2 Multiple physical, chemical, or quality properties of the sample under test are typically predicted from a single spectral measurement. In applying this practice, each property prediction is validated separately. The separate validation procedures for each property may share common features, and be affected by common effects, but the performance of each property prediction is evaluated independently. The user will typically have multiple validation procedures running simultaneously in parallel. 1.3 Results used in analyzer validation are for samples that were not used in the development of the multivariate model, and for spectra which are not outliers or nearest neighbor inliers relative to the multivariate model. 1.4 When the number, composition range or property range of available validation samples do not span the model calibration range, a local validation is done using available samples representative of current production. When the number, composition range and property range of available validation samples becomes comparable to those of the model calibration set, a general validation can be done. 1.4.1 Local Validation: 1.4.1.1 The calibration samples used in developing the multivariate model must show adequate compositional and property variation to enable the development of a meaningful correlation, and must span the compositional range of samples to be analyzed using the model to ensure that such analyses are done via interpolation rather than extrapolation. The Standard Error of Calibration (SEC) is a measure of how well the PTMRs and PPTMRs agree for this set of calibration samples. SEC includes contributions from spectrum measurement error, PTM measurement error, and model error. Sample (type) specific biases are a part of the model error. Typically, spectroscopic analyzers are very precise, so that spectral measurement error is small relative to the other types of error. 1.4.1.2 During initial analyzer validation, the compositional range of available samples may be small relative to the range of the calibration set. Because of the high precision of the spectroscopic measurement, the average difference between the PTMRs and PPTMRs may reflect a sample (type) specific bias which is statistically observable, but which are less than the 95 % uncertainty of PPTMR, U(PPTMR). Therefore, the bias and precision of the PTMR/PPTMR differences are not used as the basis for local validation. 1.4.1.3 Based on SEC, and the leverage statistic, a 95 % uncertainty for each PPTMR, U(PPTMR) is calculated. During validation, for each non-outlier sample, a determination is made as to whether the absolute difference between PPTMR and PTMR, |δ|, is less than or equal to U(PPTMR). Counts are maintained as to the total number of non-outlier validation samples, and the number of samples for which |δ| is less than or equal to U(PPTMR). Given the total number of non-outlier validation samples, an inverse binomial distribution is used to calculate the minimum number of results for which |δ| must be less than U(PPTMR). If the number of results for which |∆| is less than U(PPTMR) is greater than or equal to this minimum, then the results are consistent with the expectations of the multivariate model, and the analyzer passes local validation. The calculations involved are described in detail in Section 11 and Annex A4. 1.4.1.4 The user must establish that results that are consistent with the expectations based on the multivariate model will be adequate for the intended application. A 95 % probability is recommended for the inverse binomial distribution calculation. 1 This practice is under the jurisdiction of ASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of Subcommittee D02.25 on Performance Assessment and Validation of Process Stream Analyzer Systems. Current edition approved April 1, 2022. Published June 2022. Originally approved in 1997. Last previous edition approved in 2021 as D6122 – 21. DOI: 10.1520/D6122-22. D6122 − 22 2 The user may adjust this based on the criticality of the application. See Annex A4 for details. 1.4.2 General Validation: 1.4.2.1 When the validation samples are of sufficient number, and their compositional and property ranges are comparable to that of the model calibration set, then a General Validation can be done. 1.4.2.2 General Validation is conducted by doing a D6708 based assessment between results from the analyzer system (or subsystem) produced by application of the multivariate model, (such results are herein referred to as PPTMRs), versus the PTMRs for the same sample set. The system (or subsystem) is considered to be validated if the D6708 meets the following condition: (1) No bias correction can statistically improve the agreement between the PPTMRs versus the PTMRs, and (2) Rxy computed as per D6708 meets user-specified requirements. 1.4.2.3 For analyzers used in product release or product quality certification applications, the precision and bias requirement for the degree of agreement are typically based on the site or published precision of the PTM. NOTE 1—In most applications of this type, the PTM is the specificationcited test method. 1.4.2.4 This practice does not describe procedures for establishing precision and bias requirements for analyzer system applications. Such requirements must be based on the criticality of the results to the intended business application and on contractual and regulatory requirements. The user must establish precision and bias requirements prior to initiating the validation procedures described herein. 1.5 This practice does not cover procedures for establishing the calibration model (correlation) used by the analyzer. Calibration procedures are covered in Practice D8321 and references therein. 1.6 This practice is intended as a review for experienced persons. For novices, this practice will serve as an overview of techniques used to verify instrument performance, to verify model applicability to the spectrum of the sample under test, and to verify that the degree of agreement between PPTMRs and PTMRs meet user requirements. 1.7 This practice specifies appropriate statistical tools, outlier detection methods, for determining whether the spectrum of the sample under test is a member of the population of spectra used for the analyzer calibration. The statistical tools are used to determine if the infrared measurement results in a valid property or parameter estimate. 1.8 The outlier detection methods do not define criteria to determine whether the sample or the instrument is the cause of an outlier measurement. Thus, the operator who is measuring samples on a routine basis will find criteria to determine that a spectral measurement lies outside the calibration, but will not have specific information on the cause of the outlier. This practice does suggest methods by which instrument performance tests can be used to indicate if the outlier methods are responding to changes in the instrument response. 1.9 This practice is not intended as a quantitative performance standard for the comparison of analyzers of different design. 1.10 Although this practice deals primarily with validation of infrared and Raman analyzers, the procedures and statistical tests described herein are also applicable to other types of analyzers which employ multivariate models. 1.11 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.12 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Practice for Validation of the Performance of Multivariate Online, At-Line, Field and Laboratory Infrared Spectrophotometer, and Raman Spectrometer Based Analyzer Systems

ICS
17.180.30
CCS
发布
2022-04-01
实施

本文件规定了机动车尾气遥感检测系统的术语和定义、分类与构成、基本要求、技术要求、试验方法、检验规则、标志、包装、运输、贮存以及质量承诺。 本文件适用于利用光学原理,远距离感应测量行驶中机动车尾气排放污染物的检测系统(以下简称“遥测系统”)。

Remote sensing measurement system for motor vehicle exhaust

ICS
17.180.30
CCS
C401
发布
2022-03-28
实施
2022-04-08

本文件规定了太赫兹量子指纹中药质量控制检测分析系统的技术要求、试验方法、检验规则、标志、包装、运输和贮存方面的内容。

Terahertz quantum fingerprint detection and analysis system for quality control of traditional chinese medicine

ICS
17.180.30
CCS
C4090
发布
2022-02-28
实施
2022-03-01

1.1 This practice covers the description of requirements of spectrophotometric performance, especially for test methods, and the testing of the adequacy of available equipment for a specific method (for example, qualification for a given application). The tests give a measurement of some of the important parameters controlling results obtained in spectrophotometric methods, but it is specifically not to be concluded that all the factors in instrument performance are measured, or in fact may be required for a given application. 1.1.1 This practice is primarily directed to dispersive spectrophotometers used for transmittance measurements rather than instruments designed for diffuse transmission and diffuse reflection. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. 1 This practice is under the jurisdiction of ASTM Committee E13 on Molecular Spectroscopy and Separation Science and is the direct responsibility of Subcommittee E13.01 on Ultra-Violet, Visible, and Luminescence Spectroscopy. Current edition approved Jan. 1, 2022. Published January 2022. Originally approved in 1965. Last previous edition approved in 2013 as E275 – 08 (2013). DOI: 10.1520/E0275-08R22. Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. 1 8QLYHUVLW\RI7RURQWR 8QLYHUVLW\RI7RURQWR SXUVXDQWWR/LFHQVH$JUHHPHQW1RIXUWKHUUHSURGXFWLRQVDXWKRUL]HG 'RZQORDGHGSULQWHGE\ &RS\ULJKWE\$670,QW O DOOULJKWVUHVHUYHG 6DW-DQ*07 2. Referenced Documents

Standard Practice for Describing and Measuring Performance of Ultraviolet and Visible Spectrophotometers

ICS
17.180.30
CCS
发布
2022-01-01
实施

Method of measurement for specular glossiness

ICS
17.180.30
CCS
发布
20211231
实施
20211231

本文件规定了红外测油仪(以下简称测油仪)的要求、试验方法、检验规则、标志、包装、运输与贮存。 本文件适用于采用红外分光光度法测量固体、气体及水体中油类含量的测油仪。此仪器分为实验室、便携式、在线式3种类型。

Infrared oil gauge

ICS
17.180.30
CCS
C402
发布
2021-12-29
实施
2021-12-31

本文件规定了产品的术语和定义、要求、试验方法、检验规则及标志、包装、运输、贮存等方面的要求。 本文件适用于全自动高速旋光仪(以下简称仪器)。

High speed automatic polarimeter

ICS
17.180.30
CCS
C401
发布
2021-11-18
实施
2022-11-22

1.1 This practice2 covers the calibration of transmission densitometers used to perform measurements of diffuse optical density on radiographic films (see Note 1). 1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. NOTE 1—For further information on the design and use of densitometers, the following literature is suggested as additional background information: ISO 5–1:2009, ISO 5–2:2009, ISO 5–3:2009, and ISO 14807:2001. 1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Practice for Calibration of Transmission Densitometers

ICS
17.180.30
CCS
发布
2021-11-01
实施

1.1 This practice provides a way of specifying the angular and spatial conditions of measurement and angular selectivity of a method of measuring the spectral reflectance factors of opaque gonioapparent materials, for a small number of sets of geometric conditions. 1.2 Measurements to characterize the appearance of retroreflective materials are of such a special nature that they are treated in other ASTM documents and are not included in the scope of this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Practice for Specifying the Geometry of Multiangle Spectrophotometers

ICS
17.180.30
CCS
发布
2021-10-01
实施

Standard Practice for Performance-Based Qualification of Spectroscopic Analyzer Systems

ICS
17.180.30
CCS
发布
2021-10-01
实施

1.1 This practice describes two levels of tests to measure the performance of laboratory Fourier transform mid-infrared (FT-MIR) spectrometers equipped with a standard sample holder used for transmission measurements. 1.2 This practice is not directly applicable to Fourier transform infrared (FT-IR) spectrometers equipped with various specialized sampling accessories such as flow cells or reflectance optics, nor to Fourier transform near-infrared (FT-NIR) spectrometers, nor to FT-IR spectrometers run in step scan mode. 1.2.1 If the specialized sampling accessory can be removed and replaced with a standard transmission sample holder, then this practice can be used. However, the user should recognize that the performance measured may not reflect that which is achieved when the specialized accessory is in use. 1.2.2 If the specialized sampling accessory cannot be removed, then it may be possible to employ a modified version of this practice to measure spectrometer performance. The user is referred to Guide E1866 for a discussion of how these tests may be modified. 1.2.3 Spectrometer performance tests for FT-NIR spectrometers are described in Practice E1944. 1.2.4 Performance tests for dispersive MIR instruments are described in Practice E932. 1.2.5 For FT-IR spectrometers run in a step scan mode, variations on this practice and information provided by the instrument vendor should be used. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3.1 Exception—Informational inch-pound units are provided in 5.4. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Practice for Describing and Measuring Performance of Fourier Transform Mid-Infrared (FT-MIR) Spectrometers: Level Zero and Level One Tests

ICS
17.180.30
CCS
发布
2021-09-01
实施

1.1 This practice describes procedures for estimating the spectral bandwidth of a spectrophotometer in the wavelength region of 185 to 820 nm. 1.2 These practices are applicable to all modern spectrophotometer designs utilizing computer control and data handling. This includes conventional optical designs, where the sample is irradiated by monochromatic light, and ‘reverse’ optic designs coupled to photodiode arrays, where the light is separated by a polychromator after passing through the sample. For spectrophotometers that utilize servo-operated slits and maintain a constant period and a constant signal-to-noise ratio as the wavelength is automatically scanned, and/or utilize fixed slits and maintain a constant servo loop gain by automatically varying gain or dynode voltage, refer to the procedure described in Annex A1. This procedure is identical to that described in earlier versions of this practice. 1.3 This practice does not cover the measurement of limiting spectral bandwidth, defined as the minimum spectral bandwidth achievable under optimum experimental conditions. 1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Practice for Estimation of the Spectral Bandwidth of Ultraviolet-Visible Spectrophotometers

ICS
17.180.30
CCS
发布
2021-07-01
实施

1.1 This practice covers the procedure for certifying continuous opacity monitors. In the main part of this practice, it includes design and performance specifications, test procedures, and quality assurance requirements to ensure that continuous opacity monitors meet minimum design and calibration requirements, necessary in part, for accurate opacity monitoring measurements in regulatory environmental opacity monitoring applications subject to 10 % or higher opacity standards. In Annex A1, additional or alternative specifications are provided for certifying opacity monitors intended for use in applications where the opacity standard is less than 10 %, or where the user expects the opacity to be less than 10 % and elects to use the more restrictive criteria in Annex A1. In both cases, the error budgets for the opacity measurements are given in Appendix X1. 1.2 This practice applies specifically to the original manufacturer, or to those involved in the repair, remanufacture, or resale of opacity monitors. 1.3 Test procedures that specifically apply to the various equipment configurations of component equipment that comprise either a transmissometer, an opacity monitor, or complete opacity monitoring system are detailed in this practice. 1.4 The specifications and test procedures contained in the main part of this practice have been adopted by reference by the United States Environmental Protection Agency (U.S.EPA). For each opacity monitor or monitoring system that the manufacturer demonstrates conformance to this practice, the manufacturer may issue a certificate that states that opacity monitor or monitoring system conforms with all of the applicable design and performance requirements of 40 CFR 60, Appendix B, Performance Specification 1 except those for which tests are required after installation

Standard Practice for Opacity Monitor Manufacturers to Certify Conformance with Design and Performance Specifications

ICS
17.180.30
CCS
发布
2021-07-01
实施

  Scope is not provided for this standard

Ophthalmic instruments – Impression and applanation tonometers – Part 2 – Test methods

ICS
17.180.30
CCS
发布
2021-07-01
实施

1.1 This practice covers the description of requirements of spectrophotometric performance, especially for test methods, and the testing of the adequacy of available equipment for a specific method (for example, qualification for a given application). The tests give a measurement of some of the important parameters controlling results obtained in spectrophotometric methods, but it is specifically not to be concluded that all the factors in instrument performance are measured, or in fact may be required for a given application. 1.1.1 This practice is primarily directed to dispersive spectrophotometers used for transmittance measurements rather than instruments designed for diffuse transmission and diffuse reflection. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Practice for Describing and Measuring Performance of Ultraviolet and Visible Spectrophotometers

ICS
17.180.30
CCS
发布
2021-07-01
实施

This Standard specifies requirements for the design compliance and construction of impression and applanation tonometers, which are used for the determination of the intraocular pressure (IOP) in clinical applications. When referring to applanation tonometers, which measure the force necessary to applanate the cornea over a given diameter using the flat contact side of a pressure body, this Standard covers the method developed by Hans Goldmann.

Ophthalmic instruments – Impression and applanation tonometers – Part 1 – Metrological and technical requirements

ICS
17.180.30
CCS
发布
2021-07-01
实施

  Scope is not provided for this standard

Ophthalmic instruments – Impression and applanation tonometers – Part 3 – Test report format

ICS
17.180.30
CCS
发布
2021-07-01
实施

1.1?This practice covers requirements for the validation of measurements made by laboratory, field, or process (online or at-line) infrared (near- or mid-infrared analyzers, or both), and Raman analyzers, used in the calculation of physical, chemical, or quality parameters (that

Standard Practice for Validation of the Performance of Multivariate Online, At-Line, Field and Laboratory Infrared Spectrophotometer, and Raman Spectrometer Based Analyzer Systems

ICS
17.180.30
CCS
发布
2021-05-01
实施

1.1 This practice covers two levels of tests to measure the performance of laboratory Fourier transform near infrared (FT-NIR) spectrometers. This practice applies to the shortwave near infrared region, approximately 800 nm (12 500 cm–1 ) to 1100 nm (9090.91 cm–1 ); and the longwavelength near infrared region, approximately 1100 nm (9090.91 cm–1 ) to 2500 nm (4000 cm–1 ). This practice is intended mainly for transmittance measurements of gases and liquids, although it is broadly applicable for reflectance measurements. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Practice for Describing and Measuring Performance of Laboratory Fourier Transform Near-Infrared (FT-NIR) Spectrometers: Level Zero and Level One Tests

ICS
17.180.30
CCS
发布
2021-04-01
实施

1.1 This guide covers basic procedures that can be used to develop spectrophotometer performance tests. The guide is intended to be applicable to spectrophotometers operating in the ultraviolet, visible, near-infrared and mid-infrared regions. 1.2 This guide is not intended as a replacement for specific practices such as Practices E275, E925, E932, E958, E1421, or E1683 that exist for measuring performance of specific types of spectrophotometers. Instead, this guide is intended to provide guidelines in how similar practices should be developed when specific practices do not exist for a particular spectrophotometer type, or when specific practices are not applicable due to sampling or safety concerns. This guide can be used to develop performance tests for on-line process spectrophotometers. 1.3 This guide describes univariate level zero and level one tests, and multivariate level A and level B tests which can be implemented to measure spectrophotometer performance. These tests are designed to be used as rapid, routine checks of spectrophotometer performance. They are designed to uncover malfunctions or other changes in instrument operation, but do not specifically diagnose or quantitatively assess the malfunction or change. The tests are not intended for the comparison of spectrophotometers of different manufacture. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Guide for Establishing Spectrophotometer Performance Tests

ICS
17.180.30
CCS
发布
2021-04-01
实施



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