81.060.30 高级陶瓷 标准查询与下载

T/CSTM 00443-2023 单根纤维拉伸性能测试方法 天平法

本文件规定了利用高精度天平称量载荷法逐步增加压缩载荷测试单根纤维拉伸弹性模量的原理、仪器、样品制备、试验步骤、结果与计算和试验报告等内容。 本文件适用于单根纤维的弹性模量和拉伸强度的测试，包括金属或陶瓷纤维等纤维状材料。

Test method of the tensile properties of single fiber—Balance method

T/CSTM 00444-2023 粘结剂的粘结界面拉伸与剪切强度 试验方法 十字交叉法

本文件规定了在室温下采用十字交叉法测量不同材料或相同材料之间通过粘结剂结合后的界面拉伸和剪切强度的试验方法，并对试样制备方法、试验步骤、加载速率、数据采集和报告程序等进行了规范。 本文件适用于陶瓷砖水泥基胶粘剂、水泥混凝土界面处理剂、玻璃胶和无机高温胶，其他类型的粘结剂可参照使用。

Test method for interfacial bond strength of adhesive - Cross-bonded method

T/CSTM 00440-2023 CVD陶瓷涂层热膨胀系数和残余应力的测试方法

本文件规定了室温下CVD陶瓷涂层（厚度>0.03 mm）热膨胀系数和残余应力测试的原理，并规定了试验所需的仪器和设备、试样要求、试验步骤、数据的计算及试验报告的编写规则等。 本文件适用于在金属或陶瓷基底的CVD陶瓷涂层。本试验方法可用于材料性能研究、质量控制、特征描述以及数据采集等方向。

Test method for determining thermal expansion coefficient and residual stress of CVD ceramic coatings

ISO 5722:2023 精细陶瓷（高级陶瓷、高级工业陶瓷）.陶瓷粘合剂拉伸和剪切蠕变测定的试验方法

This document specifies a testing method for determining the tensile and shear creep of ceramic adhesive at ambient temperature by tensile and shear tests on cross-bonded test specimens. Procedures for test piece preparation, test modes, data collection, creep calculations and reporting are addressed. This document is applicable primarily to ceramic materials which are used for ceramic-ceramic, ceramic-metal and ceramic-glass joining, including monolithic fine ceramics and whisker- or particulate-reinforced ceramic composites. This test method can be used for material research, quality control, characterization and design data generation purposes.

Fine ceramics (advanced ceramics, advanced technical ceramics) — Test method for determining tensile and shear creep of ceramic adhesive

BS EN ISO 21821:2022 精细陶瓷（先进陶瓷、先进技术陶瓷）陶瓷粉末自然烧结致密化性能的测定

Fine ceramics (advanced ceramics, advanced technical ceramics). Determination of densification properties of ceramic powders on natural sintering

BS ISO 5803:2023 精细陶瓷（先进陶瓷、先进技术陶瓷） 氧化锆中单斜晶相测定的试验方法

1   Scope This document specifies a method for the qualitative and quantitative determination of the monoclinic phase present in yttria tetragonal zirconia polycrystal (Y-TZP) powders with an yttria content ≤ 6 mol% using X-ray powder diffraction. This method is also applicable for determining the monoclinic phase content in monolithic Y-TZP ceramics with an yttria content of ≤ 6 mol%. NOTE For quantitative determination of the monoclinic phase present in zirconia with a higher content of yttria or another stabilizer (e.g. MgO, CaO), this document can be referenced.

Fine ceramics (advanced ceramics, advanced technical ceramics). Test method for determination of monoclinic phase in zirconia

BS EN ISO 21814:2022 精细陶瓷（先进陶瓷、先进技术陶瓷）氮化铝粉末的化学分析方法

1   Scope This document specifies methods for the chemical analysis of fine aluminium nitride powders used as the raw material for fine ceramics. This document stipulates the determination methods of the aluminium, total nitrogen, boron, calcium, copper, iron, magnesium, manganese, molybdenum, nickel, potassium, silicon, sodium, titanium, tungsten, vanadium, zinc, zirconium, carbon, chlorine, fluorine, and oxygen contents in aluminium nitride powders. The aluminium content is determined by using either an acid pressure decomposition-CyDTA-zinc back titration method or an acid digestion-inductively coupled plasma-optical emission spectrometry (ICP-OES) method. The total nitrogen content is determined by using an acid pressure decomposition-distillation separation-acidimetric titration method, a direct decomposition-distillation separation-acidimetric titration method, or an inert gas fusion-thermal conductivity method. The boron, calcium, copper, iron, magnesium, manganese, molybdenum, nickel, potassium, silicon, sodium, titanium, tungsten, vanadium and zinc contents are determined by using an acid digestion-ICP-OES method or an acid pressure decomposition-ICP-OES method. The sodium and potassium contents are determined via an acid pressure decomposition-flame emission method or an acid pressure decomposition-atomic absorption spectrometry method. The oxygen content is determined by using an inert gas fusion-IR absorption spectrometry method, while that of carbon is determined via a combustion-IR absorption spectrometry method or a combustion-conductometry method. The chlorine and fluorine contents are determined by using a pyrohydrolysation method followed by ion chromatography or spectrophotometry.

Fine ceramics (advanced ceramics, advanced technical ceramics). Methods for chemical analysis of aluminium nitride powders

BS EN ISO 21813:2022 精细陶瓷（先进陶瓷、先进技术陶瓷）高纯钛酸钡粉末化学分析方法

Fine ceramics (advanced ceramics, advanced technical ceramics). Methods for chemical analysis of high purity barium titanate powders

BS EN ISO 20501:2022 精细陶瓷（先进陶瓷、先进技术陶瓷）强度数据的威布尔统计

1   Scope This document covers the reporting of uniaxial strength data and the estimation of probability distribution parameters for advanced ceramics which fail in a brittle fashion. The failure strength of advanced ceramics is treated as a continuous random variable. Typically, a number of test specimens with well-defined geometry are brought to failure under well-defined isothermal loading conditions. The load at which each specimen fails is recorded. The resulting failure stresses are used to obtain parameter estimates associated with the underlying population distribution. This document is restricted to the assumption that the distribution underlying the failure strengths is the two-parameter Weibull distribution with size scaling. Furthermore, this document is restricted to test specimens (tensile, flexural, pressurized ring, etc.) that are primarily subjected to uniaxial stress states. Subclauses 6.4 and 6.5 outline methods of correcting for bias errors in the estimated Weibull parameters, and to calculate confidence bounds on those estimates from data sets where all failures originate from a single flaw population (i.e. a single failure mode). In samples where failures originate from multiple independent flaw populations (e.g. competing failure modes ), the methods outlined in 6.4 and 6.5 for bias correction and confidence bounds are not applicable.

Fine ceramics (advanced ceramics, advanced technical ceramics). Weibull statistics for strength data

BS EN ISO 20504:2022 精细陶瓷（先进陶瓷、先进技术陶瓷） 陶瓷复合材料在室温下的机械性能 压缩性能的测定

1   Scope This document describes procedures for determination of the compressive behaviour of ceramic matrix composite materials with continuous fibre reinforcement at room temperature. This method applies to all ceramic matrix composites with a continuous fibre reinforcement, uni-directional (1D), bidirectional (2D) and tri-directional ( x D, with 2 <  x  < 3), tested along one principal axis of reinforcement or off axis conditions. This method also applies to carbon-fibre-reinforced carbon matrix composites (also known as carbon/carbon or C/C). Two cases of testing are distinguished: compression between platens and compression using grips.

Fine ceramics (advanced ceramics, advanced technical ceramics). Mechanical properties of ceramic composites at room temperature. Determination of compressive properties

ISO 5803:2023 精细陶瓷（高级陶瓷、高级工业陶瓷）氧化锆单斜相测定的试验方法

This document specifies a method for the qualitative and quantitative determination of the monoclinic phase present in yttria tetragonal zirconia polycrystal (Y-TZP) powders with an yttria content ≤ 6 mol% using X-ray powder diffraction. This method is also applicable for determining the monoclinic phase content in monolithic Y-TZP ceramics with an yttria content of ≤ 6 mol%. NOTE For quantitative determination of the monoclinic phase present in zirconia with a higher content of yttria or another stabilizer (e.g. MgO, CaO), this document can be referenced.

Fine ceramics (advanced ceramics, advanced technical ceramics) — Test method for determination of monoclinic phase in zirconia

BS ISO 3169:2023 精细陶瓷（先进陶瓷、先进技术陶瓷） 使用电感耦合等离子体光发射光谱法对氧化铝粉末中的杂质进行化学分析的方法

1   Scope This document specifies methods for the chemical analysis of impurities present in aluminium oxide powders used as a raw material for fine ceramics. Aluminium oxide powders are decomposed by acid pressure decomposition, acid decomposition or alkali fusion. The calcium, chromium, copper, iron, magnesium, manganese, potassium, silicon, sodium, titanium, zinc and zirconium contents in the test solution are determined by an inductively coupled plasma-optical emission spectrometer (ICP-OES).

Fine ceramics (advanced ceramics, advanced technical ceramics). Methods for chemical analysis of impurities in aluminium oxide powders using inductively coupled plasma-optical emission spectrometry

BS ISO 4825-1:2023 精细陶瓷（先进陶瓷、先进技术陶瓷） 金属化陶瓷基板热性能测量的测试方法 功率模块用热阻的评估

1   Scope This document specifies a method for measuring the thermal resistance between a heater chip and a cold plate with the heater chip mounted on a metalized ceramic substrate , imitating a silicon carbide (SiC) high-output power module. This measurement represents an index of the heat dissipation characteristics of a metallized ceramic substrate used in a high-output power module.

Fine ceramics (advanced ceramics, advanced technical ceramics). Test method for thermal property measurements of metalized ceramic substrates - Evaluation of thermal resistance for use in power modules

23/30456750 DC BS ISO 13915 精细陶瓷（高级陶瓷、先进技术陶瓷） 白光发光二极管用陶瓷荧光粉光学性能标准物质测试方法

BS ISO 13915. Fine ceramics (advanced ceramics, advanced technical ceramics). Test method for optical properties of ceramic phosphors for white light-emitting diodes with reference materials

ISO 3169:2023 精细陶瓷（高级陶瓷、高级工业陶瓷）.使用电感耦合等离子体发射光谱法对氧化铝粉末中杂质进行化学分析的方法

This document specifies methods for the chemical analysis of impurities present in aluminium oxide powders used as a raw material for fine ceramics. Aluminium oxide powders are decomposed by acid pressure decomposition, acid decomposition or alkali fusion. The calcium, chromium, copper, iron, magnesium, manganese, potassium, silicon, sodium, titanium, zinc and zirconium contents in the test solution are determined by an inductively coupled plasma-optical emission spectrometer (ICP-OES).

Fine ceramics (advanced ceramics, advanced technical ceramics) — Methods for chemical analysis of impurities in aluminium oxide powders using inductively coupled plasma-optical emission spectrometry

ISO 4825-1:2023 精细陶瓷（高级陶瓷、高级工业陶瓷）金属化陶瓷基片热性能测量的试验方法第1部分：功率模块用热阻的评定

This document specifies a method for measuring the thermal resistance between a heater chip and a cold plate with the heater chip mounted on a metalized ceramic substrate, imitating a silicon carbide (SiC) high-output power module. This measurement represents an index of the heat dissipation characteristics of a metallized ceramic substrate used in a high-output power module.

Fine ceramics (advanced ceramics, advanced technical ceramics) --Test method for thermal property measurements of metalized ceramic substrates — Part 1: Evaluation of thermal resistance for use in power modules

ASTM C1326-13(2023) 高级陶瓷努氏压痕硬度的标准试验方法

1.1 This test method covers the determination of the Knoop indentation hardness of advanced ceramics. In this test, a pointed, rhombic-based, pyramidal diamond indenter of prescribed shape is pressed into the surface of a ceramic with a predetermined force to produce a relatively small, permanent indentation. The surface projection of the long diagonal of the permanent indentation is measured using a light microscope. The length of the long diagonal and the applied force are used to calculate the Knoop hardness which represents the material’s resistance to penetration by the Knoop indenter. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 Units—When Knoop and Vickers hardness tests were developed, the force levels were specified in units of gramsforce (gf) and kilograms-force (kgf). This standard specifies the units of force and length in the International System of Units (SI); that is, force in newtons (N) and length in mm or µm. However, because of the historical precedent and continued common usage, force values in gf and kgf units are occasionally provided for information. This test method specifies that Knoop hardness be reported either in units of GPa or as a dimensionless Knoop hardness number. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Test Method for Knoop Indentation Hardness of Advanced Ceramics

ASTM C1684-18(2023) 环境温度下高级陶瓷弯曲强度的标准试验方法圆柱杆强度

1.1 This test method is for the determination of flexural strength of rod-shaped specimens of advanced ceramic materials at ambient temperature. In many instances it is preferable to test round specimens rather than rectangular bend specimens, especially if the material is fabricated in rod form. This method permits testing of machined, drawn, or as-fired rod-shaped specimens. It allows some latitude in the rod sizes and cross section shape uniformity. Rod diameters between 1.5 and 8 mm and lengths from 25 to 85 mm are recommended, but other sizes are permitted. Four-point-1⁄4-point as shown in Fig. 1 is the preferred testing configuration. Three-point loading is permitted. This method describes the apparatus, specimen requirements, test procedure, calculations, and reporting requirements. The method is applicable to monolithic or particulateor whisker-reinforced ceramics. It may also be used for glasses. It is not applicable to continuous fiberreinforced ceramic composites. 1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Test Method for Flexural Strength of Advanced Ceramics at Ambient Temperature—Cylindrical Rod Strength

ASTM C1495-16(2023) 表面磨削对高级陶瓷弯曲强度影响的标准试验方法

1.1 This test method covers the determination of the effect of surface grinding on the flexure strength of advanced ceramics. Surface grinding of an advanced ceramic material can introduce microcracks and other changes in the near surface layer, generally referred to as damage (see Fig. 1 and Ref. (1)).2 Such damage can result in a change—most often a decrease—in flexure strength of the material. The degree of change in flexure strength is determined by both the grinding process and the response characteristics of the specific ceramic material. This method compares the flexure strength of an advanced ceramic material after application of a user-specified surface grinding process with the baseline flexure strength of the same material. The baseline flexure strength is obtained after application of a surface grinding process specified in this standard. The baseline flexure strength is expected to approximate closely the inherent strength of the material. The flexure strength is measured by means of ASTM flexure test methods. 1.2 Flexure test methods used to determine the effect of surface grinding are C1161 Test Method for Flexure Strength of Advanced Ceramics at Ambient Temperatures and C1211 Test Method for Flexure Strength of Advanced Ceramics at Elevated Temperatures. 1.3 Materials covered in this standard are those advanced ceramics that meet criteria specified in flexure testing standards C1161 and C1211. 1.4 The flexure test methods supporting this standard (C1161 and C1211) require test specimens that have a rectangular cross section, flat surfaces, and that are fabricated with specific dimensions and tolerances. Only grinding processes that are capable of generating the specified flat surfaces, that is, planar grinding modes, are suitable for evaluation by this method. Among the applicable machine types are horizontal and vertical spindle reciprocating surface grinders, horizontal and vertical spindle rotary surface grinders, double disk grinders, and tool-and-cutter grinders. Incremental cross-feed, plunge, and creep-feed grinding methods may be used. 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Test Method for Effect of Surface Grinding on Flexure Strength of Advanced Ceramics

EN ISO 20501:2022 细陶瓷(高级陶瓷、高级工业陶瓷).强度数据的维伯统计

This document covers the reporting of uniaxial strength data and the estimation of probability distribution parameters for advanced ceramics which fail in a brittle fashion. The failure strength of advanced ceramics is treated as a continuous random variable. Typically, a number of test specimens with well-defined geometry are brought to failure under well-defined isothermal loading conditions. The load at which each specimen fails is recorded. The resulting failure stresses are used to obtain parameter estimates associated with the underlying population distribution. This document is restricted to the assumption that the distribution underlying the failure strengths is the two-parameter Weibull distribution with size scaling. Furthermore, this document is restricted to test specimens (tensile, flexural, pressurized ring, etc.) that are primarily subjected to uniaxial stress states. Subclauses 6.4 and 6.5 outline methods of correcting for bias errors in the estimated Weibull parameters, and to calculate confidence bounds on those estimates from data sets where all failures originate from a single flaw population (i.e. a single failure mode). In samples where failures originate from multiple independent flaw populations (e.g. competing failure modes), the methods outlined in 6.4 and 6.5 for bias correction and confidence bounds are not applicable.

Fine ceramics (advanced ceramics, advanced technical ceramics) - Weibull statistics for strength data (ISO 20501:2019)