71.060.10 化学元素 标准查询与下载



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Testing of carbonaceous materials - Determination of chemical composition - Part 1: Sample preparation, solid materials, solid binders and impregnants

ICS
71.060.10
CCS
Q50
发布
2008-01
实施

This test method provides for the determination of moisture and residue in liquid chlorine. The concentration levels of these impurities are important factors in many commercial uses of liquid chlorine.1.1 This test method covers the determination of moisture and residue in liquid chlorine. Lower limits of detection of 10 μg/g based on a 150-mL sample are achievable. 1.2 This test method describes operations and special apparatus for sampling liquid chlorine from cylinders. Sampling other commercial facilities such as tank cars, barges, and storage tanks require special techniques of manipulation in filling sample cylinders for testing. If conditions and facilities are favorable, the analysis apparatus may be connected directly to these larger storage and transportation units and on-the-spot tests may be completed. 1.3 The analytical methods are empirical and are gravimetric. They are applicable to the determination of the residue and moisture content of commercial grades of liquid chlorine (condensed gaseous product). 1.4 Residue is defined as being those substances which remain in the sample flask after sample volatilization under the conditions of the test. Moisture is defined as the volatile substances evolved during volatilization and purging of the sample-residue flask and absorbed on the desiccant contained in the absorption tubes under the conditions of the test. Some of the volatile chlorinated hydrocarbons may also be evolved from the sample residue flask during purge and absorbed, thus contributing to the apparent moisture analysis value. 1.5 This test method may be used for determining the moisture content only of gaseous chlorine if suitable and appropriate modifications are made for sample measurement and calculation. 1.6 Review the current material safety data sheet (MSDS) for detailed information concerning toxicity, first aid procedures, and safety precautions. 1.7 The values stated in inch-pound units are to be regarded as the standard. No other units of measurement are included in this standard. 1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 7.

Standard Test Method for Moisture and Residue in Liquid Chlorine

ICS
71.060.10
CCS
A43
发布
2008
实施

The round robin testing on which the precision and bias for this test method have been determined employed a range of graphites (see Table 2) whose grain sizes were of the order of 1 mil to ¼ in. (0.0254 to 6.4 mm) and larger. This wide range of carbons and graphites can be tested with uniform gauge diameters with minimum parasitic stresses to provide quality data for use in engineering applications rather than simply for quality control. This test method can be easily adapted to elevated temperature testing of carbons and graphites without changing the specimen size or configuration by simply utilizing elevated temperature materials for the load train. This test method has been utilized for temperatures as high as 4352°F (2400°C). The design of the fixtures (Figs. 2-9 and Table 1) and description of the procedures are intended to bring about, on the average, parasitic stresses of less than 5 %. The specimens for the different graphites have been designed to ensure fracture within the gauge section commensurate with experienced variability in machining and testing care at different facilities. The constant gauge diameter permits rigorous analytical treatment. 5.2 Carbon and graphite materials exhibit significant physical property differences within parent materials. Exact sampling patterns and grain orientations must be specified in order to make meaningful tensile strength comparisons. See also Test Methods C565.1.1 This test method covers the testing of carbon and graphite in tension to obtain the tensile stress-strain behavior, to failure, from which the ultimate strength, the strain to failure, and the elastic moduli may be calculated as may be required for engineering applications. Table 2 lists suggested sizes of specimens that can be used in the tests. Note 18212;The results of about 400 tests, on file at ASTM as a research report, show the ranges of materials that have been tested, the ranges of specimen configurations, and the agreement between the testers. See Section 11. Note 28212;For safety considerations, it is recommended that the chains be surrounded by suitable members so that at failure all parts of the load train behave predictably and do not constitute a hazard for the operator. 1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard. Conversions are not provided in the tables and figures. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Tensile Stress-Strain of Carbon and Graphite

ICS
71.060.10
CCS
Q51
发布
2008
实施

It is very difficult to exclude sample contamination by ambient air during the process of sampling. The levels of atmospheric contamination caused by poor sampling methods are often equal to or larger than the levels of the gaseous impurities present in the chlorine. This results in markedly elevated levels of detected impurities. As specifications become tighter, it becomes more important to measure the gaseous impurity levels in liquid chlorine correctly. Additional problems are experienced in the sampling of liquefied gases for the gaseous impurities. The gaseous impurities reach an equilibrium between the liquid phase and vapor phase in a sample bomb. The quantity of gases measured in any particular sample containing both liquid and vapor will be a function of the amount of vapor space in the sample bomb. This test method avoids the presence of liquid in the sample bomb.1.1 This test method covers sampling and analysis of liquid chlorine for the determination of oxygen (200 to 400 μg/g), nitrogen (400 to 800 μg/g), and carbon dioxide (800 to 1000 ppm) content at levels normally seen in liquid chlorine. Hydrogen and carbon monoxide concentrations in liquid chlorine are typically at or below the detection limit of this test method. Note 18212;The minimum detection limit of hydrogen using a 1 cm3 gas sample and argon carrier gas is 100 to 200 μg/g. The detection limit for the other components is significantly lower. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 Review the current Material Safety Data Sheets (MSDS) for detailed information concerning toxicity, first aid procedures, and safety precautions. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 7.

Standard Test Method for Sampling and Analysis of Liquid Chlorine for Gaseous Impurities

ICS
71.060.10
CCS
G13
发布
2008
实施

이 규격은 알루미늄 제조에 사용되는 플루오르화 나트륨에서 철 정량을 위한 1,10-페난트롤

Sodium fluoride primarily used for the production of aluminium-Determination of iron content-1,10-phenanthroline photometric method

ICS
71.060.10
CCS
G10
发布
2007-11-28
实施
2007-11-28

この規格は,繊維状活性炭の試験方法について規定する。

Test methods for fibrous activated carbon

ICS
71.060.10
CCS
G13
发布
2007-11-20
实施

この規格は,工業用の活性炭の試験方法について規定する。この規格では,粒径が150μm未満のものを粉末活性炭,粒径が150 μm以上のものを粒状活性炭とする。

Test methods for activated carbon

ICS
71.060.10
CCS
G13
发布
2007-06-20
实施

This standard describes the procurement of granular activated carbon (GAC) reactivation services and the use of reactivated GAC for water treatment. This standard does not cover the design of activated carbon handling facilities, reactivation facilities, or adsorption processes. Background information on GAC reactivation can be found ill references listed in the bibliography to this standard (appendix A).

Reactivation of Granular Activated Carbon

ICS
71.060.10
CCS
G13
发布
2007-01-21
实施
2007-06-01

This standard specifies the xylene method for the determination of density of solid carbonaceous materials.

Testing of carbonaceous materials - Determination of density by the xylene method - Solid materials

ICS
71.060.10
CCS
Q50
发布
2006-11
实施

This standard describes sodium aluminate (NaAlO) in both liquid and solid form for use in water supply service. Sodium aluminate according to this standard is a combination of sodium oxide (Na0) and aluminum oxide (Al0) with sufficient excess causticity (sodium oxide) for stabilization.

Sodium Aluminate

ICS
71.060.10
CCS
G13
发布
2006-06-11
实施
2006-12-01

The document specifies a method for the determination of flexural strength of carbonaceous materials (solid matters) by four point method.

Testing of carbonaceous materials - Determination of flexural strength by four point method - Solid materials, Corrigendum to DIN 51944:1999-01

ICS
71.060.10
CCS
Q50
发布
2006-06
实施

Testing of carbonaceous materials - Determination of flexural strength by four point method - Soild materials Corrigendum 1 to English version of DIN 51944:1999-01

ICS
71.060.10
CCS
Q50
发布
2006-06
实施

The method is used for the preparation of extruded samples of calcinated cokes.

Testing of carbonaceous materials - Preparation of extruded samples of calcinated cokes - Solid materials

ICS
71.060.10
CCS
Q50
发布
2006-04
实施

この規格は,高圧ガス容器に充てんした工業用の酸素(液化酸素及び圧縮酸素)(以下,酸素という。)について規定する。

Oxygen

ICS
71.060.10
CCS
G86
发布
2006-02-20
实施

This standard describes carbon dioxide (CO) for use in recarbonation and pH adjustment in water supply service.

Carbon Dioxide

ICS
71.060.10
CCS
G13
发布
2006-02-12
实施
2006-10-01

1.1 This Test Method covers the determination of 58 trace elements in plutonium (Pu) metal. The Pu sample is dissolved in acid, and the concentration of the trace impurities are determined by Inductively Coupled Plasma-Mass Spectroscopy (ICP-MS).1.2 This Test Method is specific for the determination of trace impurities in Pu metal. It may be applied to other types of Pu materials, such as Pu oxides, if the samples are dissolved and oxidized to the Pu(IV) state. However, it is the responsibility of the user to evaluate the performance of other matrices.This standard does not purport to address all of the safety concerns associated with its use. It is the responsibility of the user of this method to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use of this standard.

Standard Test Method for the Determination of Impurities in Plutonium Metal: Acid Digestion and Inductively Coupled Plasma-Mass Spectroscopy (ICP-MS) Analysis

ICS
71.060.10
CCS
发布
2006-01-01
实施

This standard specifies a method for the determination of dynamic modules of elasticity of carbonaceous materials (solid materials) by pulse exitation.

Testing of carbonaceous materials - Determination of dynamic moduls of elasticity by pulse excitation - Solid materials, Corrigenda to DIN 51942:2002-03

ICS
71.060.10
CCS
Q52
发布
2006-01
实施

This test method covers the determination of the thermal diffusivity of carbons and graphite to 5 % at temperatures up to 500C. It requires only a small easily fabricated specimen. Thermal diffusivity values in the range from 0.04 to 2.0 cm/s are readily measurable by this test method; however, for the reason outlined in Section 5, for materials outside this range this test method may require modification. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Test Method for Thermal Diffusivity of Carbon and Graphite by a Thermal Pulse Method

ICS
71.060.10
CCS
Q51
发布
2005-11-29
实施

この規格は,高圧ガス容器に充てんした工業用のアルゴン(液化アルゴン及び圧縮アルゴン)(以下,アルゴンという。)について規定する。

Argon

ICS
71.060.10
CCS
G86
发布
2005-10-20
实施

この規格は,高圧ガス容器に充てんした工業用の窒素(液化窒素及び圧縮窒素)(以下,窒素という。)について規定する。

Nitrogen

ICS
71.060.10
CCS
G86
发布
2005-10-20
实施



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