83.040.20 (Rubber compounding ingredients) 标准查询与下载



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These test methods are suitable for the determination of volatile material in rubber compounding materials. The test methods may be used for quality control, product acceptance, or research and development. Classification D4676 prescribes percent volatile material as an important characteristic of rubber antidegradants.1.1 These test methods cover the determination of the loss of volatile materials in various rubber chemicals based on the mass loss upon heating at 70°C. 1.2 These test methods for the determination of volatile matter include the following materials: Section Sulfur7-14 p-Phenylenediamine antidegradants15-23 1.3 The values stated in SI units are to regarded as the standard. The values given in parentheses are for information only. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Methods for Rubber Compounding Materialsmdash;Determination of Volatile Material

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G34
发布
2006
实施

This test method is designed to determine the nitrogen content of oligomeric 2,2,4-trimethyl-1,2-dihydroquinoline (TMQ) antioxidant. TMQ is used for heat protection of vulcanized rubber. This test method is suitable for assessing product specifications since nitrogen content is related to product performance, that is, antioxidant efficiency and heat protection. For comparison of product quality at different production facilities sufficient interlaboratory accuracy and precision are required.1.1 This test method covers the determination of the nitrogen content of polymerized 2,2,4-trimethyl-1,2-dihydroquinoline (TMQ). It is based on a potentiometric titration of an acetone solution of TMQ with perchloric acid in acetic acid.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 9.

Standard Test Method for Rubber Compounding Materials8212;Determination of the Basic Nitrogen Content in Rubber Antioxidant: Polymerized TMQ

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G34
发布
2006
实施

The major portion of carbon black consumed by the rubber industry is used to improve the physical properties, life expectancy, and utility of rubber products. These test methods provide an SBR recipe and directions for evaluating all types of carbon black intended for use in rubber products. Other procedures are available elsewhere in the ASTM standards for the evaluation of carbon black itself. These test methods may be used to characterize carbon black in terms of specific properties of the standard compound. These test methods are useful for the quality assurance of carbon black production. They may also be used for the preparation of reference compounds, to confirm the day-to-day reliability of testing operations used in the rubber industry, for the evaluation of experimental compounds, and quality control of production compounds.1.1 These test methods cover the standard materials, test formula, mixing procedure, and test methods for the evaluation and production control of carbon blacks in styrene butadiene rubber (SBR).1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Methods for Carbon Black in SBR (Styrene-Butadiene Rubber)-Recipe and Evaluation Procedures

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G34
发布
2006
实施

Sampling of bulk shipments of carbon blacks is of utmost importance since the location and number of samples taken by different laboratories can have a significant effect on the agreement of test values obtained. This practice is for use in obtaining representative samples of carbon black in each compartment or in the entire hopper car or hopper truck. These samples may be used to ascertain the average quality or the uniformity of a shipment, or both.1.1 This practice covers procedures for the sampling and data reporting of bulk shipments of carbon black in three-compartment hopper rail cars and compartmented bulk hopper trailers. Note 1 - The tests to be made on the samples obtained by this practice, how many samples are taken, where they are taken, and what statistical values (if any) to report shall be determined by agreement between the purchaser and the manufacturer. This practice gives guidance for use in developing such agreements or for use when no formal agreement exists. The specific details of each procedure are described in appropriate ASTM test methods used for testing carbon black.Note 2 - Some purchasers or manufacturers may consider Flexible Intermediate Bulk Containers (FIBC) to be a bulk shipment. See Practice D 1799 for guidance on sampling and reporting for this package.12. The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Practice for Carbon BlackSampling Bulk Shipments

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G49
发布
2006
实施

Sampling of bulk shipments of carbon blacks is of utmost importance since the location and number of samples taken by different laboratories can have a significant effect on the agreement of test values obtained. This practice is for use in obtaining representative samples of carbon black in each compartment or in the entire hopper car or hopper truck. These samples may be used to ascertain the average quality or the uniformity of a shipment, or both.1.1 This practice covers procedures for the sampling and data reporting of bulk shipments of carbon black in three-compartment hopper rail cars and compartmented bulk hopper trailers. Note 1 - The tests to be made on the samples obtained by this practice, how many samples are taken, where they are taken, and what statistical values (if any) to report shall be determined by agreement between the purchaser and the manufacturer. This practice gives guidance for use in developing such agreements or for use when no formal agreement exists. The specific details of each procedure are described in appropriate ASTM test methods used for testing carbon black.Note 2 - Some purchasers or manufacturers may consider Flexible Intermediate Bulk Containers (FIBC) to be a bulk shipment. See Practice D 1799 for guidance on sampling and reporting for this package.12. The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Practice for Carbon Black-Sampling Bulk Shipments

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G49
发布
2006
实施

1.1 This guide covers a procedure for using ASTM Standard Reference Blacks (SRBs) to continuously monitor the precision of those carbon black test methods for which standard values have been established. It also offers guidelines for troubleshooting various test methods.1.2 This guide establishes the x-chart control limits to be used when continuously monitoring those tests listed in Section . Alternatively, these control limits may be used as a basis for comparison to testing precision computed within a laboratory.1.3 This guide uses statistical control chart methodology as discussed in STP-15-D to determine if a laboratory's test results differ significantly from the accepted values of the SRBs.1.4 This guide provides a statistical procedure for improving test reproducibility when a laboratory cannot physically calibrate its apparatus to obtain the standard values of the ASTM SRBs, within the ranges given in the precision statement of the test method.1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Guide for Carbon Black-Validation of Test Method Precision and Bias

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G49
发布
2006
实施

These guidelines are intended to ensure that IRBs are evaluated by a standard procedure. These guidelines are to be used to establish the average physicochemical and physical rubber properties of a lot of carbon black to be used as an IRB.1.1 This practice covers guidelines for the production and testing for uniformity of a lot of carbon black to be used as an Industry Reference Black (IRB).1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Practice for Carbon Black-Evaluation of an Industry Reference Black

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G49
发布
2006
实施

These test methods are suitable for the determination of volatile material in rubber compounding materials. The test methods may be used for quality control, product acceptance, or research and development. Classification D 4676 prescribes percent volatile material as an important characteristic of rubber antidegradants.1.1 These test methods cover the determination of the loss of volatile materials in various rubber chemicals based on the mass loss upon heating at 70176;C.1.2 These test methods for the determination of volatile matter include the following materials:SectionSulfur7-14p-Phenylenediamine antidegradents15-231.3 The values stated in SI units are to regarded as the standard. The values given in parentheses are for information only.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Methods for Rubber Compounding Materials8212;Determination of Volatile Material

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G34
发布
2006
实施

Test Method A is commonly used for quality control testing because of the solvent efficiency of carbon disulfide. Test Method B employs toluene as a solvent because it is less toxic and less volatile than carbon disulfide. Test Method B is more likely to be used for research and development or for any other purpose where such information may be useful.1.1 These test methods cover the determination of solvent insoluble materials in a sulfur sample. The two test methods available are: (1) Test Method A, Extraction by Carbon Disulfide, and (2) Test Method B, Extraction by Toluene. If there are no other solvent insoluble materials present in the sulfur, these test methods determine the insoluble sulfur content directly. If other materials are also present, additional testing is necessary to identify what portion of the insolubles is insoluble sulfur.1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific warning, see 5.1.

Standard Test Methods for Rubber Chemicals8212;Determination of Percent Sulfur by Extraction

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G40
发布
2006
实施

These test methods are suitable for the determination of the ash content of rubber compounding materials. The test methods may be used for quality control, product acceptance, or research and development. Classification prescribes percent ash as an important characteristic of rubber antidegradants.1.1 These test methods cover the determination of ash content of rubber chemicals. 1.2 The test methods include the following materials: MaterialSection Sulfur 7-13 p-Phenylenediamine Antioxidants14-22 Benzothiazole Sulfenamide Accelerators14-22 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Methods for Rubber Compounding Materialsmdash;Determination of Ash Content

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G34
发布
2006
实施

1.1 This practice covers guidelines for the production and testing for uniformity of a set of carbon blacks to be used as Standard Reference Blacks (SRBs).1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Practice for Carbon Black8212;Evaluation of Standard Reference Blacks

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G49
发布
2005
实施

This test method may be used as a raw material quality-control tool.1.1 This test method covers a practical test for the solubility of commercial chemicals used in rubber products. 1.2 It is not a true measure of solubility, since equilibrium is not approached from both sides, that is, higher temperature and lower temperature. 1.3 The test method indicates the total solubility, under the conditions of the test, of all components in the presence of each other and in the proportions present in the sample. 1.4 This test method does not measure the solubility of a rubber chemical in rubber. 1.5 The values stated in SI units are to be considered standard. 1.6 This standard does not purport to address the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Rubber Chemicals8212;Solubility

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G34
发布
2005
实施

1.1 This practice covers guidelines for the production and testing for uniformity of a set of carbon blacks to be used as Standard Reference Blacks (SRBs).1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Practice for Carbon Black8212;Evaluation of Standard Reference Blacks

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G49
发布
2005
实施

1.1 This practice covers guidelines for the production and testing for uniformity of a set of carbon blacks to be used as Standard Reference Blacks (SRBs).1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Practice for Carbon Black8212;Evaluation of Standard Reference Blacks

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G49
发布
2005
实施

Pellet hardness is related to several carbon black characteristics. Among these are mass strength and attrition. The subsequent level of dispersion obtained in some mixed compounds containing the carbon black may be affected by pellet hardness. Acceptable pellet hardness must be agreed to by the user and the producer. Note 18212;Test Method D 5230 is the preferred standard for testing of individual pellet hardness. It is recognized that Test Method D 3313 relies on operator judgement, thus adding an additional source of variation for this test.1.1 This test method covers a method for measuring the hardness of individual pellets of carbon black.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Carbon Black8212;Individual Pellet Hardness

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G49
发布
2005
实施

Individual pellet hardness is related to several carbon black characteristics. Among these are mass strength and attrition. The subsequent level of dispersion obtained in some mixed compounds containing the carbon black may be affected by pellet hardness. Acceptable pellet hardness must be agreed to by the user and the producer.1.1 This test method covers a procedure for measuring individual pellet hardness of carbon black by the automated pellet hardness tester.1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Carbon Black8212;Automated Individual Pellet Hardness

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G49
发布
2005
实施

1.1 This practice covers guidelines for the production and testing for uniformity of a lot of carbon black to be used as an Industry Reference Black (IRB).1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Practice for Carbon Black-Evaluation of an Industry Reference Black

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G49
发布
2005
实施

MBT is commonly used as an accelerator for rubber and latex vulcanization. The purity of MBT may be of importance in predicting performance in rubber compounds and this test method is designed to assess the purity of MBT. This test method may be used as a quality control tool and for research and development work.1.1 This test method covers a procedure for the assay of 2-mercaptobenzothiazole (MBT). It is based on a potentiometric titration of MBT with sodium hydroxide. 1.2 The assay is determined as percent by mass. 1.3 The values given in SI units are to be regarded as standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Rubber Chemicals8212;2-Mercaptobenzothiazole (MBT)8212;Assay

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G34
发布
2005
实施

1.1 This test method covers a method for measuring the hardness of individual pellets of carbon black.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Carbon Black8212;Individual Pellet Hardness

ICS
83.040.20 (Rubber compounding ingredients)
CCS
G49
发布
2005
实施

Pour density is a function of the degree of compaction during pelletization. It is strongly influenced by and inversely proportional to structure (OAN). Pour density of carbon black is useful for estimating the weight-to-volume relationship for certain applications, such as automatic batch loading systems, and for estimating weights of bulk shipments. 1.1 This test method covers the determination of the pour density of pelleted carbon blacks. 1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Carbon Black, Pelleted8212;Pour Density

ICS
83.040.20 (Rubber compounding ingredients)
CCS
发布
2005
实施



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