A43 化学 标准查询与下载



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1.1 This is a compilation of terms commonly used in analytical chemistry for metals, ores, and related materials. Terms that are generally understood or defined adequately in other readily available sources are either not included or their sources are identified. 1.2 A definition is a single sentence with additional information included in a Discussion. 1.3 Definitions identical to those published by another standards organization or ASTM committee are identified with the name of the organization or the identifying document and ASTM committee. 1.4 Definitions specific to a particular field (such as emission spectroscopy ) are identified with an italicized introductory phrase.

Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials

ICS
01.040.71 (Chemical technology (Vocabularies)); 71
CCS
A43
发布
1999
实施

1.1 This test method is intended for use with digested samples that were collected originally during the abatement of lead hazards from buildings and related structures. 1.2 This test method covers the lead analysis of sample digestates (for example, digested paint, soil, dust, and airborne particulate) using inductively coupled plasma atomic emission spectrometry (ICP-AES), flame atomic absorption spectrometry (FAAS), and graphite furnace atomic absorption spectrometry (GFAAS) techniques. 1.3 No detailed operating instructions can be provided because of differences among various makes and models of satisfactory instruments. Instead, the analyst should follow the instructions provided by the manufacturer of the particular instrument. 1.4 This test method contains directions for sample analysis as well as quality assurance (QA) and quality control (QC) and may be used for purposes of laboratory accreditation and certification. 1.5 The use of analytical instrumentation other than ICP-AES, FAAS, and GFAAS is not within the scope of this test method. 1.6 The values stated in SI units are to be regarded as the standard. 1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Determination of Lead by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES), Flame Atomic Absorption Spectrometry (FAAS), or Graphite Furnace Atomic Absorption Spectrometry (GFAAS) Techniques

ICS
77.120.60 (Lead, zinc, tin and their alloys)
CCS
A43
发布
1999
实施

1.1 These practices cover the techniques most often used in infrared quantitative analysis. Practices associated with the collection and analysis of data on a computer are included as well as practices that do not use a computer. 1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements appear in Section 6 and Notes A4.7, A4.11, and A5.5.

Standard Practices for General Techniques of Infrared Quantitative Analysis

ICS
71.040.50 (Physicochemical methods of analysis)
CCS
A43
发布
1999
实施

This test method provides for the determination of moisture and residue in liquid chlorine. The concentration levels of these impurities are important factors in many commercial uses of liquid chlorine.1.1 This test method covers the determination of moisture and residue in liquid chlorine. Lower limits of detection of 10 ppm (w/w) based on a 150 mL sample are achievable. 1.2 This test method describes operations and special apparatus for sampling liquid chlorine from cylinders. Sampling other commercial facilities such as tank cars, barges, and storage tanks require special techniques of manipulation in filling sample cylinders for testing. If conditions and facilities are favorable, the analysis apparatus may be connected directly to these larger storage and transportation units and on-the-spot tests may be completed. 1.3 The analytical methods are empirical and are gravimetric. They are applicable to the determination of the residue and moisture content of commercial grades of liquid chlorine (condensed gaseous product). 1.4 Residue is defined as being those substances which remain in the sample flask after sample volatilization under the conditions of the test. Moisture is defined as the volatile substances evolved during volatilization and purging of the sample-residue flask and absorbed on the desiccant contained in the absorption tubes under the conditions of the test. Some of the volatile chlorinated hydrocarbons may also be evolved from the sample residue flask during purge and absorbed, thus contributing to the apparent moisture analysis value. 1.5 This test method may be used for determining the moisture content only of gaseous chlorine if suitable and appropriate modifications are made for sample measurement and calculation. 1.6 The values stated in inch-pound units are to be regarded as the standard. The metric equivalents of inch-pound units may be approximate. 1.7 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 7.

Standard Test Method for Moisture and Residue in Liquid Chlorine

ICS
71.060.10 (Chemical elements)
CCS
A43
发布
1998
实施

1.1 This test method covers the determination of mercury in liquid chlorine with a lower limit of detection of 0.1 ppb. 1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 7, 6.3, 6.4, 6.5, and Note 2.

Standard Test Method for Mercury in Liquid Chlorine

ICS
CCS
A43
发布
1998
实施

1.1 This test method covers the determination of sulfur in organic compounds by sodium peroxide bomb ignition. It is intended for application to samples of organic materials containing more than 0.5% sulfur. The presence of iron may require a separation such as is described. 1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use . For specific hazard statements, see Section 7 and Notes 2 and 3. Note 1-A test method based on an oxygen bomb combustion of petroleum products is described in Test Method D129.

Standard Test Method for Sulfur in Organic Compounds by Sodium Peroxide Bomb Ignition

ICS
CCS
A43
发布
1998
实施

1.1 This practice presents procedures and statistics for an interlaboratory study (ILS) of the performance of an analytical method. The study provides statistical values which are useful in determining if a method is satisfactory for the purposes for which it was developed. These statistical values may be incorporated in the method's precision and bias section. This practice discusses the meaning of the statistics and what users of analytical methods may learn from them. 1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method

ICS
71.040.40 (Chemical analysis)
CCS
A43
发布
1998
实施

1.1 This practice covers a procedure for the determination of microgram per millilitre ([mu]g/mL) or lower concentrations of elements in solution using an electrothermal atomization device attached to an atomic absorption spectrophotometer. A general description of the equipment is provided. Recommendations are made for preparing the instrument for measurements, establishing optimum temperature conditions and other criteria which should result in determining a useful calibration concentration range, and measuring and calculating the test solution analyte concentration. 1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific safety hazard statements are given in Section 9. Note 1-This practice is a companion to Practice E663.

Standard Practice for Electrothermal (Graphite Furnace) Atomic Absorption Analysis

ICS
71.040.50 (Physicochemical methods of analysis)
CCS
A43
发布
1998
实施

This test method was developed primarily for the determination of traces of mercury in chlorine produced by the mercury-cell process.1.1 This test method covers the determination of mercury in liquid chlorine with a lower limit of detection of 0.1 ppb.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Sections 7, 6.3, 6.4, 6.5, and Note 2.1.3 Review the current safety data sheet (MSDS) for detailed information concerning toxicity, first-aid procedures, and safety precautions.

Standard Test Method for Mercury in Liquid Chlorine

ICS
71.040.40 (Chemical analysis); 71.060.10 (Chemical
CCS
A43
发布
1998
实施

1.1 This test method covers the determination of moisture and residue in liquid chlorine. Lower limits of detection of 10 ppm (w/w) based on a 150 mL sample are achievable. 1.2 This test method describes operations and special apparatus for sampling liquid chlorine from cylinders. Sampling other commercial facilities such as tank cars, barges, and storage tanks require special techniques of manipulation in filling sample cylinders for testing. If conditions and facilities are favorable, the analysis apparatus may be connected directly to these larger storage and transportation units and on-the-spot tests may be completed. 1.3 The analytical methods are empirical and are gravimetric. They are applicable to the determination of the residue and moisture content of commercial grades of liquid chlorine (condensed gaseous product). 1.4 Residue is defined as being those substances which remain in the sample flask after sample volatilization under the conditions of the test. Moisture is defined as the volatile substances evolved during volatilization and purging of the sample-residue flask and absorbed on the desiccant contained in the absorption tubes under the conditions of the test. Some of the volatile chlorinated hydrocarbons may also be evolved from the sample residue flask during purge and absorbed, thus contributing to the apparent moisture analysis value. 1.5 This test method may be used for determining the moisture content only of gaseous chlorine if suitable and appropriate modifications are made for sample measurement and calculation. 1.6 The values stated in inch-pound units are to be regarded as the standard. The metric equivalents of inch-pound units may be approximate. 1.7 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 7.

Standard Test Method for Moisture and Residue in Liquid Chlorine

ICS
CCS
A43
发布
1998
实施

This test method may be used to determine the total sulfur content of unknown organic samples or to assay known sulfur containing organic compounds. This test method may be used on organic materials in which the complete conversion of sulfur to sulfate can be accomplished by sodium peroxide bomb ignition. This test method assumes that sulfate is quantitatively measured by precipitation with barium chloride solution.1.1 This test method covers the determination of sulfur in organic compounds by sodium peroxide bomb ignition. It is intended for application to samples of organic materials containing more than 0.5 % sulfur. The presence of iron may require a separation such as is described.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see 6.6.2, Section 7 and 8.3. Note 18212;A Test method baseed on an oxygen bomb combustion of petroleum products is described in Test Method D 129.1.3 Review the current Material Safety Data Sheets (MSDS) for detailed information concerning toxicity, first aid procedures, and safety precautions.

Standard Test Method for Sulfur in Organic Compounds by Sodium Peroxide Bomb Ignition

ICS
71.040.40;71.060.20
CCS
A43
发布
1998
实施

This test method is applicable to the determination of phosphorus in organic materials containing at least 1.0 % phosphorus. It can be used as an assay procedure for known phosphorus organic compounds.1.1 This test method covers the determination of phosphorus in organic compounds by sodium peroxide bomb ignition. It is applicable to samples of organic materials containing more than 1.0 % phosphorus.1.2 The values stated in SI units are to be regarded as the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8, and Note , Note , and Note .1.4 Review the current material safety data sheets (MSDS) for detailed information concerning toxicity, first-aid procedures; and safety precautions.

Standard Test Method for Phosphorus in Organic Compounds by Sodium Peroxide Bomb Ignition

ICS
71.040.50;71.080.01
CCS
A43
发布
1998
实施

1.1 This test method is intended to provide a general technique incorporating thermogravimetry to determine the amount of highly volatile matter, medium volatile matter, combustible material, and ash content of compounds. This test method will be useful in performing a compositional analysis in cases where agreed upon by interested parties. 1.2 This test method is applicable to solids and liquids. 1.3 The temperature range of test is typically room temperature to 1000176C. Composition between 1 and 100 weight% of individual components may be determined. 1.4 This test method utilizes an inert and reactive gas environment. 1.5 Computer or electronic-based instruments, techniques, or data treatment equivalent to this method may also be used. Users of this test method are expressly advised that all such instruments or techniques may not be equivalent. It is the responsibility of the user of this test method to determine the necessary equivalency prior to use. In the case of dispute, only the manual procedures described in this test method are to be considered valid. 1.6 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use .

Standard Test Method for Compositional Analysis by Thermogravimetry

ICS
71.040.40 (Chemical analysis)
CCS
A43
发布
1998
实施

Ideally, interlaboratory testing of a method is carried out by a randomly chosen group of laboratories that typifies the kind of laboratory that is likely to use the method. In actuality, this ideal is only approximated by the laboratories that are available and willing to undertake the test work. The coordinator of the program must ensure that every participating laboratory has appropriate facilities and personnel and performs the method exactly as written. If this goal is achieved, the statistics developed during the ILS will be adequate for determining if the method is capable of producing satisfactory precision in actual use. If the program includes certified reference materials, the test data also provide information concerning the accuracy of the method. The statistics provide a general guide to the expected performance of the method in the laboratories of those who will use it.1.1 This practice presents procedures and statistics for an interlaboratory study (ILS) of the performance of an analytical method. The study provides statistical values which are useful in determining if a method is satisfactory for the purposes for which it was developed. These statistical values may be incorporated in the method's precision and bias section. This practice discusses the meaning of the statistics and what users of analytical methods may learn from them. 1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method

ICS
71.040.40 (Chemical analysis)
CCS
A43
发布
1998
实施

This test method may be used to determine the total chlorine content of unknown organic samples or to assay known chlorine containing organic compounds. This test method may be used on organic materials in which the complete conversion to chloride can be accomplished by sodium peroxide bomb ignition, and which contain no other halogens.1.1 This test method covers the determination of chlorine in organic compounds by sodium peroxide bomb ignition. It is intended for application to samples of organic materials containing more than 0.5 % chlorine. The procedure assumes that compounds containing halogens other than chlorine will not be present.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific safety precautions, see 6.5.2, Section 7, 8.3, and 8.9.1.3 Review the current Material Safety Data Sheets (MSDS) for detailed information concerning toxicity, first aid procedures, and safety precautions.Note 18212;Other test methods based on oxygen bomb combustion for analysis for chlorine are described in Test Method D 808, Test Method D 2361, and Test Method D 4208.

Standard Test Method for Chlorine in Organic Compounds by Sodium Peroxide Bomb Ignition

ICS
71.040.40 (Chemical analysis); 71.060.20 (Oxides)
CCS
A43
发布
1998
实施

1.1 This test method covers the determination of chlorine in organic compounds by sodium peroxide bomb ignition. It is intended for application to samples of organic materials containing more than 0.5% chlorine. The procedure assumes that compounds containing halogens other than chlorine will not be present. 1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use . For specific safety precautions, see Section 7 and Notes 2, 3, and 4. Note 1-Other test methods based on oxygen bomb combustion for analysis for chlorine are described in Test Method D808, Test Method D2361, and Test Method D4208.

Standard Test Method for Chlorine in Organic Compounds by Sodium Peroxide Bomb Ignition

ICS
CCS
A43
发布
1998
实施

1.1 This test method covers the determination of phosphorus in organic compounds by sodium peroxide bomb ignition. It is applicable to samples of organic materials containing more than 1.0% phosphorus. 1.2 The values stated in SI units are to be regarded as the standard. 1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8, and Notes 1, 2, and 6.

Standard Test Method for Phosphorus in Organic Compounds by Sodium Peroxide Bomb Ignition

ICS
CCS
A43
发布
1998
实施

이 규격은 플로트형 면적 유량계(이하 유량계라 한다)를 사용하여 관내를 흐르는 액체, 기체

Method of measurement by variable area flowmeters

ICS
17.120.20
CCS
A43
发布
1997-12-09
实施
1997-12-09

이 규격은 관로의 지름이 50∼1200mm인 원형 관로 안을 채운 상태에서 흐르는 유체의

Measurement of fluid flow by means of orifice plates, nozzles and Venturi tubes inserted in circular cross-section conduits running full

ICS
17.120.10
CCS
A43
发布
1997-09-22
实施
1997-09-22

General rules for analytical gas chromatography methods

ICS
CCS
A43
发布
1997-01-23
实施
1997-04-01



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