G74 催化剂基础标准与通用方法 标准查询与下载

ASTM D3766-08 催化剂和催化作用的相关标准术语

1.1 This terminology covers definitions of terms related to catalysts and catalysis. Note 18212;The Manual of Symbols and Terminology for Physicochemical Quantities and Units presents authoritative descriptions of many terms used in the field of catalysis.

Standard Terminology Relating to Catalysts and Catalysis

ASTM D7442-08a 通过感应耦合等离子体-原子发射光谱测量法进行元素分析用流化床催化裂化催化剂的试样制备的标准实施规程

The chemical composition of catalyst and catalyst materials is an important indicator of catalyst performance and is a valuable tool for assessing parameters in a FCCU process. This practice will be useful to catalyst manufacturers and petroleum refiners for quality verification and performance evaluation, and to environmental authorities at the state and federal levels for evaluation and verification of various compliance programs. Catalysts and catalyst type materials are difficult to prepare for analysis by ICP, and although the techniques presented in this practice are common, there is wide variation among laboratories in sample pretreatment and digestion recipes. This practice is intended to standardize these variables in order to facilitate the utility of comparative data among manufacturers, refiners, and regulatory agencies.1.1 This practice covers uniform dissolution techniques for preparing samples of fluid catalytic cracking catalysts (FCC) and exchanged zeolitic materials for analysis by Inductively Coupled Plasma Atomic Emission Spectroscopy (ICP-AES). These techniques describe standardized approaches to well-known, widely used laboratory practices of sample preparation utilizing acid digestions and borate salt fusions. This practice is applicable to fresh and equilibrium FCC catalysts and exchanged zeolite materials. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Practice for Sample Preparation of Fluid Catalytic Cracking Catalysts and Zeolites for Elemental Analysis by Inductively Coupled Plasma Atomic Emission Spectroscopy

HG/T 2693-2007 一氧化碳高温变换催化剂化学成分分析方法

本标准规定了一氧化碳高温变换催化剂的主要化学成分的分析方法。 本标准适用于一氧化碳高温变换催化剂中铁、铬、氧化钾、总钼、本体硫和烧失量质量分数的测定。

Analytical method of chemical composition in high temperature carbon monoxide shift catalyst

HG/T 2089-2007 二氧化硫氧化制硫酸催化剂活性试验方法

本标准规定了二氧化硫氧化制硫酸催化剂活性的试验方法。 本标准适用于接触法硫酸生产过程中将二氧化硫氧化为三氧化硫的二氧化硫氧化制硫酸催化剂。

Test method of activity for oxidizing sulphuric dioxide into sulphuric acid catalyst

HG/T 2513-2006 氧化锌脱硫剂硫容试验方法

本标准规定了氧化锌脱硫剂硫容的试验方法。 本标准适用于合成氨、制氢、合成甲醇、有机合成原料气（油）中脱除硫化氢和部分有机硫化物的氧化锌脱硫剂。

Test method of zinc oxide desulfurization sorbent

HG/T 2510-2006 甲烷化催化剂活性试验方法

本标准规定了甲烷化催化剂活性的试验方法。 本标准适用于合成氨及制氢系统装置内使气体中少量碳氧化物和氢生成甲烷的甲烷化催化剂。

Test method of activity for methanation catalyst

HG/T 2514-2006 有机硫加氢催化剂活性试验方法

本标准规定了有机硫加氢催化剂活性试验方法。 本标准适用于合成氨、合成甲醇及制氢装置中所有的含钴、钼的有机硫加氢催化剂。

Test method of activity for organic sulfur hydrogenation catalyst

HG/T 3555-2006 轻油转化催化剂化学成分分析方法

本标准规定了轻油转化催化剂化学成分分析方法。 本标准适用于轻油转化催化剂中氧化镍（10%～50%）、三氧化二铝（20%～70%）、氧化钙（10%～15%）、氧化镁（10%～15%）、三氧化二铁 (0.5%～1%) 、二氧化钛(0.5%～1%) 、二氧化硅（0.5%～13%）、氧化钾（2%～6%）、二氧化锆（0.3%～1%）和烧失量质量分数的测定。

Analytical method of chemical components in light oil reforming catalyst

HG/T 3545-2006 氨合成催化剂活性试验方法

本标准规定了氨合成催化剂活性的试验方法。 本标准适用于氢和氮反应制取氨的氨合成催化剂。

Test method of activity for ammonia synthesis catalyst

HG/T 3544-2006 一氧化碳高温变换催化剂活性试验方法

本标准规定了一氧化碳高温变换催化剂活性的试验方法。 本标准适用于合成氨及制氢装置中一氧化碳加水蒸气制氢的一氧化碳高温变换催化剂。

Test method of activity for high temperature carbon monoxide shift catalyst

HG/T 2273.4-2006 天然气一、二段转化催化剂试验方法

本标准规定了天然气一、二段转化催化剂的活性和耐热性能的试验方法。 本标准适用于合成氨、甲醇及制氢装置中使用的天然气加水蒸气制氢的天然气一、二段转化催化剂。

Test method of natural gas reforming catalyst for primary and secondary reformer

HG/T 3543-2006 天然气转化催化剂化学成份分析方法

本标准规定了天然气转化催化剂化学成分的分析方法。 本标准适用于天然气转化催化剂中氧化镍、三氧化二铝、氧化钙、三氧化二镧、二氧化硅、三氧化二铁、氧化钾、氧化钠以及烧失量质量分数的测定。

Analytical method of chemical composition in natural gas reforming catalyst

ASTM D7206-06 含金属的流化裂化催化剂(FCC)的循环钝化的标准指南

This guide describes techniques of deactivation that can be used to compare a series of cracking catalysts at equilibrium conditions or to simulate the equilibrium conditions of a specific commercial unit and a specific catalyst.1.1 This guide covers the deactivation of fluid catalytic cracking (FCC) catalyst in the laboratory as a precursor to small scale performance testing. FCC catalysts are deactivated in the laboratory in order to simulate the aging that occurs during continuous use in a commercial fluid catalytic cracking unit (FCCU). Deactivation for purposes of this guide constitutes hydrothermal deactivation of the catalyst and metal poisoning by nickel and vanadium. Hydrothermal treatment is used to simulate the physical changes that occur in the FCC catalyst through repeated regeneration cycles. Hydrothermal treatment (steaming) destabilizes the faujasite (zeolite Y), resulting in reduced crystallinity and surface area. Further decomposition of the crystalline structure occurs in the presence of vanadium, and to a lesser extent in the presence of nickel. Vanadium is believed to form vanadic acid in a hydrothermal environment resulting in destruction of the zeolitic portion of the catalyst. Nickels principle effect is to poison the selectivity of the FCC catalyst. Hydrogen and coke production is increased in the presence of nickel, due to the dehydrogenation activity of the metal. Vanadium also exhibits significant dehydrogenation activity, the degree of which can be influenced by the oxidation and reduction conditions prevailing throughout the deactivation process. The simulation of the metal effects that one would see commercially is part of the objective of deactivating catalysts in the laboratory.1.2 The two basic approaches to laboratory-scale simulation of commercial equilibrium catalysts described in this guide are as follows:1.2.1 Cyclic Propylene Steaming (CPS) Methodin which the catalyst is impregnated with the desired metals via an incipient wetness procedure (Mitchell method) followed by a prescribed steam deactivation.1.2.2 Crack-on Methods in which fresh catalyst is subjected to a repetitive sequence of cracking (using a feed with enhanced metals concentrations), stripping, and regeneration in the presence of steam. Two specific procedures are presented here, a procedure with alternating metal deposition and deactivation steps and a modified Two-Step procedure, which includes a cyclic deactivation process to target lower vanadium dehydrogenation activity.1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Guide for Cyclic Deactivation of Fluid Catalytic Cracking (FCC) Catalysts with Metals

HG/T 3554-2005 氨合成催化剂化学成份分析方法

本标准规定了氨合成催化剂化学成份分析方法。 本标准适用于氨合成催化剂及其他相同组分催化剂中的总铁（Fe)、二价铁与三价铁比值（Fe+/Fe+）、氧化钾（KO）、氯化钙（CaO)、氧化镁（MgO）、三氧化二铝（AlO）、二氧化硅（SiO）、二氧化钛（TiO）、磷（P）、氧化钡（BaO）、四氧化三钴（CoO）的测定。

Analytical method of chemical composition in ammonia synthesis catalyst

HG/T 2512-2005 氧化锌脱硫剂化学成分分析方法

本标准规定了以氧化锌为主要原料的氧化锌脱硫剂化学成分分析方法。 本标准适用于氧化锌脱硫剂中的氧化锌、二氧化锰、氧化镁及烧失量质量分数的测定。

Analytical method of chemical composition in zinc oxide desulfurization sorbent

HG/T 2516-2005 二氧化硫氧化制硫酸催化剂化学成份分析方法

本标准规定了二氧化硫氧化制硫酸催化剂化学成分分析方法。 本标准适用于二氧化硫氧化制硫酸催化剂中，五氧化二钒（4%～10%）、硫酸钾（15%～25%）、硫酸钠（1%～15%）、五氧化二磷（0.5%～3.5%）、三氧化二锑（0.5%～3%）、三氧化二铁（0.2%～2%）、二氧化硅（大于50%）和烧失量质量分数的测定。

Analytical method of chemical composition in the catalyst oxidizing sulphuric dioxide into sulphuric acid

HG/T 2511-2005 甲烷化催化剂化学成分分析方法

本标准规定了甲烷化催化剂化学成分分析方法。 本标准适用于甲烷化催化剂中的镍（Ni)、三氧化二铝(AlO

Analytical method of chemical composition in methanation catalyst

HG/T 2515-2005 有机硫加氢催化剂活性组分分析方法

本标准规定了有机硫加氢催化剂中活性组分钴（Co）、三氧化钼（MoO）的分析方法。 本标准适用于有机硫加氢催化剂中的钴（Co）、三氧化钼（MoO）质量分数的测定。

Analytical method of the active composition in organic sulfur hydrogenation catalyst

HG/T 3553-2005 一氧化碳低温变换催化剂化学成份分析方法

本标准规定了一氧化碳低温变换催化剂以及化学组成相同的催化剂成份的分析方法。 本标准适用于一氧化碳低温变换催化剂中的氧化锌、氧化铜、三氧化二铝、三氧化二铁、氧化钠、烧失量质量分数的测定。

Analytical method of chemical composition in low temperature carbon monoxide shift catalyst

HG/T 3542-2005 化肥催化剂中微量硫分析方法

本标准规定了用次亚磷酸钠还原亚甲基蓝分光光度法和硫酸钡称量分析法测定化肥催化剂中微量硫的质量分数。 本标准适用于各类化肥催化剂中微量硫的质量分数的测定，其中次亚磷酸钠还原亚甲基蓝光光度法适用于硫的质量分数在0.0005%～0.1% 的硫的测定，硫酸钡称量分析法适用于硫的质量分数在0.03%～0.7% 的硫的测定

Analytical method of micro-sulphur in fertilizer catalyst