Z18 土壤环境质量分析方法 标准查询与下载

DB14/T 1949-2019 土壤卤代烃的测定 顶空/固相微萃取-气相色谱法

本标准规定了测定土壤中卤代烃的顶空/固相微萃取-气相色谱法。本标准适用于山西省境内土壤中26 种卤代烃的测定。

Determination of Soil Halogenated Hydrocarbons Headspace/Solid Phase Microextraction-Gas Chromatography

HJ 1054-2019 土壤和沉积物 二硫代氨基甲酸酯（盐）类农药总量的测定 顶空/气相色谱法

本标准规定了测定土壤和沉积物中二硫代氨基甲酸酯（盐）类农药总量的顶空/气相色谱法。 本标准适用于土壤和沉积物中二硫代氨基甲酸酯（盐）类农药总量的测定，以代森锰锌或二硫化碳计。 本标准不适用于含烃基黄原酸及其盐类土壤和沉积物样品的测定。 当取样量为2g，以代森锰锌计时，方法检出限为0.05 mg/kg，测定下限为0.20 mg/kg；以二硫化碳计时，方法检出限为0.03 mg/kg，测定下限为0.12 mg/kg。

Soil and sediment—Determination of dithiocarbamate pesticides —Headspace gas chromatography

HJ 1020-2019 土壤和沉积物 石油烃（C6-C9）的测定 吹扫捕集 气相色谱法

本标准规定了测定土壤和沉积物中石油烃（C-C9）的吹扫捕集/气相色谱法。 本标准适用于土壤和沉积物中石油烃（C6C9）的测定。 当取样量为5.0g时，本标准测定石油烃（C-Co）的方法检出限为0.04mg/kg，测定下限为0.16mg/kg。

Soil and sediment-Determination of petroleum hydrocarbons（C6-C9）-Purge and trap/gas chromatography

NY/T 3420-2019 土壤有效硒的测定 氢化物发生原子荧光光谱法

Determination of soil available selenium by hydride generation atomic fluorescence spectrometry

HJ 974-2018 土壤和沉积物 11种元素的测定 碱熔-电感耦合等离子体发射光谱法

本标准适用于土壤和沉积物中锰（Mn）、钡（Ba）、钒（V）、锶（Sr）、钛（Ti）、钙（Ca）、镁（Mg）、铁（Fe）、铝（Al）、钾（K）和硅（Si）等11 种元素的测定。

Determination of Eleven Elements in Soil and Sediment Alkali Fusion-Inductively Coupled Plasma Emission Spectrometry

DB61/T 1162-2018 土壤 重金属元素的测定 能量色散X射线荧光光谱法

本标准规定了采用能量色散 X 射线荧光光谱法测量土壤中重金属元素的方法原理 ， 设备与材料 ， 测 试方法 ， 结果计算方法等 。 本标准适用于快速测定土壤中重金属元素 （ 钛 、 钒 、 铬 、 锰 、 铁 、 钴 、 镍 、 铜 、 锌 、 镉 、 硒 、 汞 、 锑 、 砷 、 铅等 ） 种类及含量 。

Determination of Heavy Metal Elements in Soil by Energy Dispersive X-ray Fluorescence Spectrometry

HJ 960-2018 土壤和沉积物 氨基甲酸酯类农药的测定 柱后衍生-高效液相色谱法

本标准规定了测定土壤和沉积物中10 种氨基甲酸酯类农药的柱后衍生-高效液相色谱法。 本标准适用于土壤和沉积物中涕灭威亚砜、涕灭威砜、灭多威、3-羟基克百威、涕灭威、残杀威、克百威、甲萘威、异丙威、甲硫威等10 种氨基甲酸酯类农药的测定。 当取样量为10 g，试样定容体积为1.0 ml，进样体积为15 μl 时，10 种氨基甲酸酯类农药的方法检出限为1～3 μg/kg，测定下限为4～12 μg/kg。详见附录A。

Soil and sediment— Determination of carbamate pesticides—Post-column derivatization- high performance liquid chromatography

HJ 923-2017 土壤和沉积物 总汞的测定 催化热解-冷原子吸收分光光度法

本标准适用于土壤和沉积物中总汞的测定。

Soil and sediment—Determination of total mercury —Catalytic pyrolysis-cold atomic absorption spectrophotometry

HJ 873-2017 土壤 水溶性氟化物和总氟化物的测定 离子选择电极法

本标准规定了测定土壤中水溶性氟化物和总氟化物的离子选择电极法。 本标准适用于土壤中水溶性氟化物和总氟化物的测定。 当称样量为 5.0g，试样移取量为 40.0ml时，本标准测定水溶性氟化物的方法检出限为 0.7 mg/kg，测定下限为 2.8 mg/kg，测定上限为 125mg/kg；当称样量为 0.2 g，试样移取量为 20.0ml时，测定总氟化物的方法检出限为 63mg/kg，测定下限为 252mg/kg，测定上限为 1.25×104 mg/kg。

Soil-Determination of water soluble fluoride and total fluoride - Ion selective electrode method

ISO 11504:2017 土质.受石油烃污染土壤紧实度评估

Soil quality - Assessment of impact from soil contaminated with petroleum hydrocarbons

HJ 835-2017 土壤和沉积物 有机氯农药的测定 气相色谱-质谱法

本标准规定了测定土壤和沉积物中有机氯农药的气相色谱-质谱法。 本标准适用于土壤和沉积物中23种有机氯农药的测定，目标物包括：α-六六六、六氯苯、β-六六六、γ-六六六、δ-六六六、七氯、艾氏剂、环氧化七氯、α-氯丹、α-硫丹、γ-氯丹、狄氏剂、p,p＇-DDE、异狄氏剂、β-硫丹、p,p＇-DDD、硫丹硫酸酯、异狄氏剂醛、o,p＇-DDT、异狄氏剂酮、p,p＇-DDT、甲氧滴滴涕、灭蚁灵。通过验证，其他有机氯农药也可适用本标准。 当取样量为20.0g，浓缩后定容体积为1 .0 ml时，采用全扫描方式测定，方法检出限为 0.02 mg/kg~0.09 mg/kg，测定下限为0.08 mg/kg~0.36 mg/kg。详见附录A。

Soil and sediment – Determination of organochlorine pesticides– Gas chromatography/Mass spectrometry

DIN 19738:2017 土壤质量.污染的土壤材料中有机和无机污染物的生物利用度

Soil quality - Bioaccessibility of organic and inorganic pollutants from contaminated soil material

BS ISO 18400-201:2017 土壤质量. 取样. 现场物理预处理

Soil quality. Sampling. Physical pretreatment in the field

DIN EN 16171:2017 污泥,处理过的生物废弃物和土壤.利用电感耦合等离子体质谱法(ICP-MS)测定元素;德文版本EN 16171-2016

Sludge, treated biowaste and soil - Determination of elements using inductively coupled plasma mass spectrometry (ICP-MS); German version EN 16171:2016

ASTM C998-17 放射性核素用地表土取样的标准实施规程

5.1 Soil provides a source material for the determination of selected radionuclides and serves as an integrator of the deposition of airborne materials. Soil sampling should not be used as the primary measurement system to demonstrate compliance with applicable radionuclides in air standards. This should be done by air sampling or by measuring emission rates. Soil sampling does serve as a secondary system, and in many cases, is the only available avenue if insufficient air sampling occurred at the time of an incident. For many insoluble radionuclides, the primary exposure pathway to the general population is by inhalation. The resuspension of transuranic elements has received considerable attention (1, 2)4 and their measurement in soil is one means of establishing compliance with the U.S. Environmental Protection Agency (EPA) guidelines on exposure to transuranic elements. Soil sampling can provide useful information for other purposes, such as plant uptake studies, total inventory of various radionuclides in soil due to atmospheric nuclear tests, and the accumulation of radionuclides as a function of time. A soil sampling and analysis program as part of a preoperational environmental monitoring program serves to establish baseline concentrations. Consideration was given to these criteria in preparing this practice. 5.2 Soil collected using this practice and subsequent analysis can be used to monitor radionuclide deposition of emissions from nuclear facilities. The critical factors necessary to provide this information are sampling location, time of sampling, frequency of sampling, sample size, and maintenance of the integrity of the sample prior to analysis. Since the soil is considered to be a heterogeneous medium, multipoint sampling is necessary. The samples must represent the conditions existing in the area for which data are desired. FIG. 1 Soil Sampling Instrument and Use 1.1 This practice covers the sampling of surface soil for the purpose of obtaining a sample representative of a particular area for subsequent chemical analysis of selected radionuclides. This practice describes one acceptable approach to collect soil samples for radiochemical analysis. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Org......

Standard Practice for Sampling Surface Soil for Radionuclides

ASTM C1402-17 土壤样品高分辨率γ射线能谱的标准指南

5.1 Gamma-ray spectrometry of soil samples is used to identify and quantify certain gamma-ray emitting radionuclides. Use of a germanium semiconductor detector is necessary for high-resolution gamma-ray measurements. 5.2 Much of the data acquisition and analysis can be automated with the use of commercially available systems that include both hardware and software. For a general description of the typical hardware in more detail than discussed in Section 7, see Ref (19). For best practices on set-up, calibration, and quality control of utilized spectrometry systems, see Practice D7282. 5.3 Both qualitative and quantitative analyses may be performed using the same measurement data. 5.4 The procedures described in this guide may be used for a wide variety of activity levels, from natural background levels and fallout-type problems, to determining the effectiveness of cleanup efforts after a spill or an industrial accident, to tracing contamination at older production sites, where wastes were purposely disposed of in soil. In some cases, the combination of radionuclide identities and concentration ratios can be used to determine the source of the radioactive materials. 5.5 Collecting samples and bringing them to a data acquisition system for analysis may be used as the primary method to detect deposition of radionuclides in soil. For obtaining a representative set of samples that cover a particular area, see Practice C998. Soil can also be measured by taking the data acquisition system to the field and measuring the soil in place (in situ). In situ measurement techniques are not discussed in this guide. 1.1 This guide covers the identification and quantitative determination of gamma-ray emitting radionuclides in soil samples by means of gamma-ray spectrometry. It is applicable to nuclides emitting gamma rays with an approximate energy range of 20 to 2000 keV. For typical gamma-ray spectrometry systems and sample types, activity levels of about 5 Bq (135 pCi) are measured easily for most nuclides, and activity levels as low as 0.1 Bq (2.7 pCi) can be measured for many nuclides. It is not applicable to radionuclides that emit no gamma rays such as the pure beta-emitting radionuclides hydrogen-3, carbon-14, strontium-90, and becquerel quantities of most transuranics. This guide does not address the in situ measurement techniques, where soil is analyzed in place without sampling. Guidance for in situ techniques can be found in Ref (1) and (2).2 This guide also does not discuss methods for determining lower limits of detection. Such discussions can be found in Refs (3), (4), (

Standard Guide for High-Resolution Gamma-Ray Spectrometry of Soil Samples

ASTM C999-17 制备土壤样品测定放射性核素的标准实施规程

5.1 Soil samples prepared for radionuclide analyses by this practice can be used to characterize radionuclide constituents. This practice is intended to produce a homogeneous sample from which smaller aliquots may be drawn for radionuclide characterization. 5.2 Many soil characterization plans for radionuclide constituents utilize gamma-ray spectrometry measurements of soil to quantify a number of possible gamma emitting analytes. A widely used practice for these measurements is to fill a calibrated sample container, such as a Marinelli beaker (∼600-mL volume), with a homogenized soil sample for counting such as what may be done using Guide C1402. By preparing the entire soil core collection, sufficient homogeneous sample is available for such gamma-ray spectrometry and other radiochemical measurements. 1.1 This practice covers the preparation of surface soil samples collected for analysis of radionuclide constituents, particularly uranium and plutonium. This practice describes one acceptable approach to the preparation of soil samples for radiochemical analysis. 1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. A specific hazard statement is given in 7.3. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Practice for Soil Sample Preparation for the Determination of Radionuclides

DIN EN 16175-2:2016 污泥、处理的生物废物和土壤.汞的测定.第2部分:冷蒸气原子荧光光谱法(CV-AFS).德文版本EN 16175-2-2016

Sludge, treated biowaste and soil - Determination of mercury - Part 2: Cold-vapour atomic fluorescence spectrometry (CV-AFS); German version EN 16175-2:2016

DIN EN 16175-1:2016 污泥、处理的生物废物和土壤.汞的测定.第1部分:冷蒸气原子吸收光谱法(CV-AAS).德文版本EN 16175-1-2016

Sludge, treated biowaste and soil - Determination of mercury - Part 1: Cold-vapour atomic absorption spectrometry (CV-AAS); German version EN 16175-1:2016

DIN EN ISO 15009:2016 土质.气相测谱法测定挥发性芳烃、萘和挥发性卤代烃含量.热解析的吹扫捕集法(ISO 15009-2016).德文版本EN ISO 15009-2016

Soil quality - Gas chromatographic determination of the content of volatile aromatic hydrocarbons, naphthalene and volatile halogenated hydrocarbons - Purge-and-trap method with thermal desorption (ISO 15009:2016); German version EN ISO 15009:2016