1. 使用能谱安全须知
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2. 能谱仪开关机顺序
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3. 能谱仪硬件介绍
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3.1 准直器
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3.2 电子陷阱
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3.3 晶体以及场效应管
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3.4 冷指
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3.5 前置放大器
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3.6 液氮液位探测器
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3.7 X-STREAM & MICS 控制器
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4. 能谱分析原理简介
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4.1
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5. INCA软件使用指南
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5.1 Analyser
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5.2 POINT&ID
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5.3 SMARTMAP
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5.4 Feature and GSR
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6. INCA定量分析及定量技巧
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7. 试样准备
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7.1 试样制备方法
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8.
数据管理及保存···············································································································
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9.日常维护
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8.1 Auto Collection Setup 设置自动收集
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8.2 Auto Spectrum Collection 谱线的自动收集
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8.3 Processing Spectra from Disk
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10.联系我们··························································································································
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第一章 安全知识
高压危险标志! 存在有可能致人伤亡的高电压。
警告标志!若不遵守指示,可能导致仪器的损坏人身的伤害。
为防止火灾或电击:
l 如果线缆有破损,请勿使用仪器;
l 如果提供的电压超出规定范围,请勿使用仪器;
l 仪器箱盖打开时,请勿使用仪器;
l 不要在潮湿的环境中使用仪器;
l 不要将仪器浸没液体中;
l 不要在腐蚀性气体环境中使用仪器;
l 不要在超过规定温度范围使用仪器;
l 让仪器在通风良好的环境中工作,以防过热;
l 仅使用原厂提供的线缆和备件;
l 保证仪器接地良好。
安全预防点:
x-stream 控制器内含电路可产生超过1千伏的高压,不要打开该控制器,内部也没有用户需要维护的部件。
不要在计算机内再使用其他IEEE1394设备,这可能导致硬件无法工作。
若非我公司建议,不要对计算机系统盘(通常是C盘)进行重新格式化、分区、操作系统重装等工作,这会导致系统数据丢失而无法恢复。(用户对系统自行处理而造成数据丢失的,不在保修范围之内)
能谱仪的正常工作需要用户提供液氮。液态氮是惰性的,无色,无嗅,无腐蚀性,不可燃,温度极低。氮构成了大气的大部分(体积比78.03%,重量比75.5%)。液氮会导致严重冻伤,在通风不充分的设备里,小量液体汽化成大量气体造成的过压,和狭窄工作空间内的氧被取代造成的窒息。储存和使用液氮要充分通风。当操作或使用液氮时,或任何有(液氮)溢出而存在暴露的可能性的时候,都要穿戴个人防护装备(眼罩和手套)。