EN ISO 1628-2:2020
塑料.用毛细管粘度计测定稀释溶液中聚合物的粘度.第2部分:聚氯乙烯树脂

Plastics - Determination of the viscosity of polymers in dilute solution using capillary viscometers - Part 2: Poly(vinyl chloride) resins (ISO 1628-2:2020)

2021-01

EN ISO 1628-2:2020 发布历史

1.1 This document specifies conditions for the determination of the reduced viscosity (also known as viscosity number) and K-value of PVC resins. It is applicable to resins in powder form which consist of homopolymers of the monomer vinyl chloride and copolymers, terpolymers, etc., of vinyl chloride with one or more other monomers, but where vinyl chloride is the main constituent. The resins may contain small amounts of unpolymerized substances (e.g. emulsifying or suspending agents, catalyst residues, etc.) and other substances added during the course of the polymerization. This document is not applicable, however, to resins having a volatile-matter content in excess of 0,5 % ± 0,1 %, when determined in accordance with ISO 1269. In addition to this, it is not applicable to resins which are not entirely soluble in cyclohexanone. 1.2 The reduced viscosity and K-value of a particular resin are related to its molecular mass, but the relationship varies depending on the concentration and type(s) of other monomer(s) present. Hence, homopolymers and copolymers having the same reduced viscosity or K-value might not have the same molecular mass. 1.3 The values determined for reduced viscosity and K-value, for a particular sample of PVC resin, are influenced differently by the concentration of the solution chosen for the determination. Hence the use of the procedures described in this document only gives values for reduced viscosity and K-value that are comparable when the concentrations of the solutions used are identical. 1.4 Limiting viscosity number is not used for PVC resins. 1.5 The experimental procedures described in this document can also be used to characterize the polymeric fraction obtained during the chemical analysis of a PVC composition. However, the values calculated for the reduced viscosity and K-value in these circumstances might not indicate the actual values for the resin used to produce the composition because of the impure nature of the recovered polymer fraction.

EN ISO 1628-2:2020由欧洲标准化委员会 IX-CEN 发布于 2020-07-15,并于 2020-10-31 实施,于 2021-01-31 废止。

EN ISO 1628-2:2020在国际标准分类中归属于: 83.080.20 热塑性塑料。

EN ISO 1628-2:2020的历代版本如下:

  • 2020年 EN ISO 1628-2:2020 塑料.用毛细管粘度计测定稀释溶液中聚合物的粘度.第2部分:聚氯乙烯树脂
  • 1998年 EN ISO 1628-2:1998 塑料.用毛细管粘度计测定稀释溶液中聚合物的粘度.第2部分:聚氯乙烯树脂ISO 1628-2-1998

 

 

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标准号
EN ISO 1628-2:2020
发布
2020年
发布单位
欧洲标准化委员会
当前最新
EN ISO 1628-2:2020
 
 
适用范围
1.1 This document specifies conditions for the determination of the reduced viscosity (also known as viscosity number) and K-value of PVC resins. It is applicable to resins in powder form which consist of homopolymers of the monomer vinyl chloride and copolymers, terpolymers, etc., of vinyl chloride with one or more other monomers, but where vinyl chloride is the main constituent. The resins may contain small amounts of unpolymerized substances (e.g. emulsifying or suspending agents, catalyst residues, etc.) and other substances added during the course of the polymerization. This document is not applicable, however, to resins having a volatile-matter content in excess of 0,5 % ± 0,1 %, when determined in accordance with ISO 1269. In addition to this, it is not applicable to resins which are not entirely soluble in cyclohexanone. 1.2 The reduced viscosity and K-value of a particular resin are related to its molecular mass, but the relationship varies depending on the concentration and type(s) of other monomer(s) present. Hence, homopolymers and copolymers having the same reduced viscosity or K-value might not have the same molecular mass. 1.3 The values determined for reduced viscosity and K-value, for a particular sample of PVC resin, are influenced differently by the concentration of the solution chosen for the determination. Hence the use of the procedures described in this document only gives values for reduced viscosity and K-value that are comparable when the concentrations of the solutions used are identical. 1.4 Limiting viscosity number is not used for PVC resins. 1.5 The experimental procedures described in this document can also be used to characterize the polymeric fraction obtained during the chemical analysis of a PVC composition. However, the values calculated for the reduced viscosity and K-value in these circumstances might not indicate the actual values for the resin used to produce the composition because of the impure nature of the recovered polymer fraction.

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