4.1 The service life of many structural ceramic components is often limited by the subcritical growth of cracks over time, under stress at a defined temperature, and in a defined chemical environment (Refs 1-3). When one or more cracks grow to a critical size, brittle catastrophic failure may occur in the component. Slow crack growth in ceramics is commonly accelerated at elevated temperatures. This test method provides a procedure for measuring the long term load-carrying ability and appraising the relative slow crack growth susceptibility of ceramic materials at elevated temperatures as a function of time, temperature, and environment. This test method is based on Test Method C1576 with the addition of provisions for elevated temperature testing.
4.2 This test method is also used to determine the influences of processing variables and composition on slow crack growth at elevated temperatures, as well as on strength behavior of newly developed or existing materials, thus allowing tailoring and optimizing material processing for further modification.
4.3 This test method may be used for material development, quality control, characterization, design code or model verification, time-to-failure, and limited design data generation purposes.
Note 2: Data generated by this test method do not necessarily correspond to crack velocities that may be encountered in service conditions. The use of data generated by this test method for design purposes, depending on the range and magnitude of applied stresses used, may entail extrapolation and uncertainty.
4.4 This test method and Test Method C1576 are similar and related to Test Methods C1368 and C1465; however, C1368 and C1465 use constant stress-rates (linearly increasing stress over time) to determine corresponding flexural strengths, whereas this test method and C1576 employ a constant stress (fixed stress levels over time) to determine corresponding times-to-failure. In general, the data generated by this test method may be more representative of actual service conditions as compared with data from constant stress-rate testing. However, in terms of test time, constant stress testing is inherently and significantly more time consuming than constant stress-rate testing.
4.5 The flexural stress computation in this test method is based on simple elastic beam theory, with the following assumptions: the material is isotropic and homogeneous; the moduli of elasticity in tension and compression are identical; and the material is linearly elastic. These assumptions are based on small grain size in the ceramic specimens. The grain size should be no greater than 1/50 of the beam depth as measured by the mean linear intercept method (E112). In cases where the material grain size is bimodal or the grain size distribution......
对于此类实验,一般用临界应力、断裂时间或者临界氢浓度来评价材料的延迟断裂敏感性。 恒应变延迟断裂试验。恒应变延迟断裂试验是使试样处于恒定应变的受力状态下,其主要特点是简单、经济、试样紧凑,不需要特殊的装置,仅利用夹具或螺栓紧固即可获得应力。试样的实际应力随工作截面的减少而降低。一般通过测定延迟断裂试样占总试样数目的百分比或试样断裂的时间,来比较材料延迟断裂的敏感性。 慢应变速率拉伸试验。...
在注塑过程中,如果使用水分含量过多的塑料粒子进行生产,则会产生一些加工问题,并最终影响成品质量,如:表面开裂、反光,以及抗冲击性能和拉伸强度等机械性能降低等。三、熔融指数熔融指数:是一种表示塑胶材料加工时的流动性的数值。测试方法:先让塑料粒在一定时间(10分钟)内、一定温度及压力(各种材料标准不同)下,融化成塑料流体,然后通过一直径圆管所流出的重量或体积。...
测试设备:马沸炉测试方法:煅烧法(燃烧有机物并在高温下处理其残余物直至恒重),在马沸炉里,600℃进行10min燃烧,称量其残留物。...
测试标准GB/T.1040-2006 塑料拉伸性能的测定 GB/T.2918-1998 塑料试样状态调节和试验的标准环境GB/T.17200-2008 橡胶塑料拉力、压力和弯曲试验机(恒速驱动)技术规范GB/T.1043.1-2008 塑料简支梁冲击性能的测定 第1部分:非仪器化冲击GB/T.1843-2008 塑料悬臂梁冲击强度的测定GB/T.9871-2008 硫化橡胶或热塑性橡胶老化性能的测定拉伸应力松弛试验...
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