E44 石油焦 标准查询与下载

ASTM D4931-06(2011) 新出炉的石油焦炭中总含水量的标准试验方法

Moisture adds weight to the coke and serves no useful purpose. A knowledge of the moisture content is important in the purchase and sale of green petroleum coke, both of which are conducted on a dry basis. The collection of the sample as specified for the Drying Oven Method is intended for the express purpose of determining the total moisture of green petroleum coke. The standard is available to producers, sellers, and consumers for determination when other techniques or modifications are not mutually agreed on. The Preparation Procedure is used only when sample contains free water. Obtaining a representative sample of a coke source is compounded by the presence of free water.1.1 This test method covers both the preparation procedure for samples containing free water (air drying loss (ADL) on gross moisture samples) and the determination of the gross moisture content of green petroleum coke. 1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Gross Moisture in Green Petroleum Coke

ASTM D4930-06(2011) 锻烧石油焦用防尘材料的标准试验方法

The test is designed to quantify the amount of dust control material added to calcined coke. The dust control material is applied to calcined coke to help maintain a dust-free environment. It generally serves no other useful purpose. It adds weight to the coke and can have a negative effect on the quality of carbon and graphite artifacts made from the treated coke. For these reasons the coke customer wants to know the amount of dust control material on the coke and can specify a maximum level.1.1 This test method covers the determination of the amount of material applied to calcined coke to control dust associated with coke handling and transportation. 1.2 This test method is limited to those materials that are soluble in a solvent that can be used in a Soxhlet extraction type of apparatus such as methylene chloride (dichloro-methane). Note 18212;Methylene chloride is the most popular solvent for removing dust control oil at the time this procedure is being written. Toluene and methyl chloroform, however, have been used with equal results on all cokes tested which have included only those sprayed with aromatic or waxy materials. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Section 7.

Standard Test Method for Dust Control Material on Calcined Petroleum Coke

ASTM D5003-06a(2011) 石油焦的哈德格罗夫可磨性指数(HGI)的标准试验方法

The HGI is used to predict the ranking of raw petroleum cokes or calcined petroleum cokes in industrial size mills used for crushing operations. The rankings are based on energy required and feed rate or both. The HGI is also used to select raw petroleum cokes and coals that are compatible with each other when milled together in a blend so that segregation of the blend does not occur during particle size reduction.1.1 This test method covers the determination of the hardgrove grindability index (HGI) of those petroleum cokes that contain no dedusting additive. The procedure for this test method is the same as in Test Method D409. Sections of this test method contain the significance and use of the HGI of petroleum coke, preliminary sample preparation procedures, and procedure and precision and bias data specific to petroleum coke. Note 18212;The size consistency (particle size distribution) of fluid petroleum coke is generally 100 % passing a 6.73 mm (No. 3) sieve and greater than 80 % passing a 2.00 mm (No. 10) sieve. Much of fluid cokes will pass a 0.59 mm (No. 30) sieve. Because of this fineness the HGI value is related to the coarser particles in fluid coke and large samples are required to prepare sufficient material of the correct particle size for Test Method D409. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.2.1 Exception8212;Hardgrove grindability index is unitless. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Hardgrove Grindability Index (HGI) of Petroleum Coke

ASTM D6376-06 利用波长色散X射线荧光光谱学测定石油焦中痕量金属的标准试验方法

The presence and concentration of sulfur and various metallic elements in a petroleum coke are major factors determining the suitability of a coke for various purposes. This test method provides rapid means for measuring sulfur and commercially important metallic elements in coke samples. This test method provides a guide for determining conformance to material specifications for use by buyers and sellers in a commercial transfer of petroleum coke. Sulfur contents can be used to evaluate the potential formation of sulfur oxides (SOx), a source of atmospheric pollution. 1.1 This test method covers the X-ray fluorescence spectrometric determination of total sulfur and trace metals in samples of raw or calcined petroleum coke. Elements determined using this test method are listed in Table 1.1.2 Detection limits, sensitivity, and optimal element ranges will vary with matrices, spectrometer type, analyzing crystal, and other instrument conditions and parameters.1.3 All analytes are determined as the element and reported as such. These include all elements listed in Table 1. This test method may be applicable to additional elements or concentration ranges if sufficient standards are available to produce proper calibration equations.1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Determination of Trace Metals in Petroleum Coke by Wavelength Dispersive X-Ray Fluorescence Spectroscopy

ASTM D2638-06 氦比重瓶测定煅烧石油焦真密度的标准试验方法

The real density of calcined petroleum coke directly influences the physical and chemical properties of the manufactured carbon and graphite artifacts for which it is used. Density, therefore, is a major quality specification of calcined petroleum coke and is used as a control in coke calcination.1.1 This test method covers the determination of the real density (RD) of calcined petroleum coke. Real density, by definition is obtained when the particle size of the specimen is smaller than 75 microns (No. 200 Sieve).1.2 The values stated in acceptable metric units are to be regarded as the standard.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Real Density of Calcined Petroleum Coke by Helium Pycnometer

ASTM D4930-06 煅烧石油焦用防尘材料的标准试验方法

The test is designed to quantify the amount of dust control material added to calcined coke. The dust control material is applied to calcined coke to help maintain a dust-free environment. It generally serves no other useful purpose. It adds weight to the coke and can have a negative effect on the quality of carbon and graphite artifacts made from the treated coke. For these reasons the coke customer wants to know the amount of dust control material on the coke and can specify a maximum level.1.1 This test method covers the determination of the amount of material applied to calcined coke to control dust associated with coke handling and transportation.1.2 This test method is limited to those materials that are soluble in a solvent that can be used in a Soxhlet extraction type of apparatus such as methylene chloride (dichloro-methane).Note 18212;Methylene chloride is the most popular solvent for removing dust control oil at the time this procedure is being written. Toluene and methyl chloroform, however, have been used with equal results on all cokes tested which have included only those sprayed with aromatic or waxy materials.1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 7.

Standard Test Method for Dust Control Material on Calcined Petroleum Coke

ASTM D4931-06 新出炉的石油焦炭中总含水量的标准试验方法

Moisture adds weight to the coke and serves no useful purpose. A knowledge of the moisture content is important in the purchase and sale of green petroleum coke, both of which are conducted on a dry basis. The collection of the sample as specified for the Drying Oven Method is intended for the express purpose of determining the total moisture of green petroleum coke. The standard is available to producers, sellers, and consumers for determination when other techniques or modifications are not mutually agreed on. The Preparation Procedure is used only when sample contains free water. Obtaining a representative sample of a coke source is compounded by the presence of free water.1.1 This test method covers both the preparation procedure for samples containing free water (air drying loss (ADL) on gross moisture samples) and the determination of the gross moisture content of green petroleum coke.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Gross Moisture in Green Petroleum Coke

BS EN 14639:2005 原焦油和原苯.特性和试验方法

This European Standard defines the methods of tests for the determination of the characteristics of crude tar and crude benzole.

Crude tar and crude benzole - Characteristics and test methods

ASTM D6376-05 利用波长色散X射线荧光光谱学测定石油焦中痕量金属的标准试验方法

1.1 This test method covers the X-ray fluorescence spectrometric determination of total sulfur and trace metals in samples of raw or calcined petroleum coke. Elements determined using this test method are listed in Table 1. 1.2 Detection limits, sensitivity, and optimal element ranges will vary with matrices, spectrometer type, analyzing crystal, and other instrument conditions and parameters. 1.3 All analytes are determined as the element and reported as such. These include all elements listed in Table 1. This test method may be applicable to additional elements or concentration ranges if sufficient standards are available to produce proper calibration equations. 1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Determination of Trace Metals in Petroleum Coke by Wavelength Dispersive X-Ray Fluorescence Spectroscopy

CAS 105-2004 煅烧石油焦

本标准规定了煅烧石油普通焦的分类、要求、试验方法、标志、包装、运输及贮存。 本标准适用于以延迟石油焦为生产原料，经过1250℃以上的高温煅烧后制成的煅烧石油普通焦。

Calcined petroleum coke

CAS 104-2004 煅烧石油针状焦

本标准规定了煅烧石油针状焦的分类、要求、试验方法、标志、包装、运输及贮存。 本标准适用于以延迟焦化装置生产的，经过1300℃以上的高温煅烧后制成的煅烧石油针状焦。

Calcined petroleum needle coke

ASTM D5600-04 感应耦合等离子体原子发射光谱法(ICP-AES)分析石油焦炭中痕量金属的标准试验方法

1.1 This test method covers the analysis for commonly determined trace metals in test specimens of raw and calcined petroleum coke by inductively coupled plasma atomic emission spectroscopy.1.2 Elements for which this test method is applicable are listed in . Detection limits, sensitivity, and optimum ranges of the metals will vary with the matrices and model of spectrometer.1.3 This test method is applicable only to samples containing less than one mass % ash.1.4 Elements present at concentrations above the upper limit of the working ranges can be determined with additional, appropriate dilutions.1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Trace Metals in Petroleum Coke by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)

ASTM D5600-04e1 感应耦合等离子体原子发射光谱法(ICP-AES)分析石油焦炭中痕量金属的标准试验方法

The presence and concentration of various metallic elements in a petroleum coke are major factors in determining the suitability of the coke for various end uses. This test method provides a means of determining the concentrations of these metallic elements in a coke sample. The test method provides a standard procedure for use by buyer and seller in the commercial transfer of petroleum coke to determine whether the petroleum coke meets the specifications of the purchasing party.1.1 This test method covers the analysis for commonly determined trace metals in test specimens of raw and calcined petroleum coke by inductively coupled plasma atomic emission spectroscopy.1.2 Elements for which this test method is applicable are listed in . Detection limits, sensitivity, and optimum ranges of the metals will vary with the matrices and model of spectrometer.1.3 This test method is applicable only to samples containing less than one mass % ash.1.4 Elements present at concentrations above the upper limit of the working ranges can be determined with additional, appropriate dilutions.1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Trace Metals in Petroleum Coke by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)

ASTM D5056-04(2010) 原子吸收法测定石油焦炭中痕量金属的标准试验方法

The presence and concentration of various metallic elements in a petroleum coke are major factors in the suitability of the coke for various uses. This test method provides a means of measuring the amounts of those metallic elements in the coke sample. The test method provides a standard procedure for use by the purchaser and seller in the commercial transfer of petroleum coke to determine whether the lot of coke meets the specifications of the purchasing party.1.1 This test method covers the analysis for the commonly determined trace metals (aluminum, calcium, iron, nickel, silicon, sodium, and vanadium) in laboratory analysis samples of raw and calcined petroleum coke by atomic absorption spectroscopy. 1.2 The elemental concentration ranges for which this test method is applicable and the limits of detection of this test method are listed in Table 1. 1.3 The values stated in SI units are to be regarded as the standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Trace Metals in Petroleum Coke by Atomic Absorption

ASTM D5056-04 用原子吸收法测定石油焦炭中痕量金属的标准试验方法

The presence and concentration of various metallic elements in a petroleum coke are major factors in the suitability of the coke for various uses. This test method provides a means of measuring the amounts of those metallic elements in the coke sample. The test method provides a standard procedure for use by the purchaser and seller in the commercial transfer of petroleum coke to determine whether the lot of coke meets the specifications of the purchasing party.1.1 This test method covers the analysis for the commonly determined trace metals (aluminum, calcium, iron, nickel, silicon, sodium, and vanadium) in laboratory analysis samples of raw and calcined petroleum coke by atomic absorption spectroscopy.1.2 The elemental concentration ranges for which this test method is applicable and the limits of detection of this test method are listed in Table 1.1.3 The values stated in SI units are to be regarded as the standard.1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For hazard statements, see Sections 8-10.

Standard Test Method for Trace Metals in Petroleum Coke by Atomic Absorption

ASTM D6969-03 分析用焙烧石油焦样品准备的标准规程

This practice provides field personnel and laboratories with standard procedures for dividing, reducing, and mixing gross samples and intermediate samples, such that the resulting prepared analysis samples are more uniform from laboratory to laboratory. Adherence to these guidelines is expected to provide significant reduction in inter-laboratory variability.1.1 This practice covers the preparation procedures necessary for the reduction and division of calcined petroleum coke samples in order to generate appropriate analytical samples upon which physical and chemical analytical tests will be performed.1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Practice for Preparation of Calcined Petroleum Coke Samples for Analysis

ASTM D4422-03 石油焦炭分析中灰分的标准试验方法

The ash content is one of the properties used to evaluate petroleum coke and indicates the amount of undesirable residue present. Acceptable ash content varies with the intended use.1.1 This test method covers the determination of the ash content of petroleum coke.1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Ash in Analysis of Petroleum Coke

ASTM D6969-03(2008) 分析用焙烧石油焦样品准备的标准实施规程

This practice provides field personnel and laboratories with standard procedures for dividing, reducing, and mixing gross samples and intermediate samples, such that the resulting prepared analysis samples are more uniform from laboratory to laboratory. Adherence to these guidelines is expected to provide significant reduction in interlaboratory variability.1.1 This practice covers the preparation procedures necessary for the reduction and division of calcined petroleum coke samples in order to generate appropriate analytical samples upon which physical and chemical analytical tests will be performed. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Practice for Preparation of Calcined Petroleum Coke Samples for Analysis

ASTM D6970-03(2008) 分析用焙烧石油焦样品收集的标准实施规程

Data obtained from calcined petroleum coke samples are used in commercial transactions, controlling plant operations, and allocating production costs. Use of standard sampling procedures facilitates the task of obtaining a sample to represent an entire lot of calcined petroleum coke. This practice gives general procedures for the collection of calcined petroleum coke samples and is intended to provide useful methodology for the collection of a sample to represent a lot of calcined petroleum coke. The variety of calcined petroleum coke handling facilities and sampling applications preclude the publication of detailed procedures for every sampling situation.1.1 This practice covers procedures for the collection of calcined petroleum coke samples from conveyor belts or transfer points. These samples may be used for physical and chemical analyses. 1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Practice for Collection of Calcined Petroleum Coke Samples for Analysis

ASTM D4422-03(2008) 石油焦炭分析中灰分的标准试验方法

The ash content is one of the properties used to evaluate petroleum coke and indicates the amount of undesirable residue present. Acceptable ash content varies with the intended use.1.1 This test method covers the determination of the ash content of petroleum coke. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standard Test Method for Ash in Analysis of Petroleum Coke