ASTM D2622-2003
波长分散X射线荧光光谱法测定石油产品中硫含量的标准试验方法

Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry

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标准号

ASTM D2622-2003

发布日期

2003年

实施日期

废止日期

无

中国标准分类号

E30

国际标准分类号

75.080 (Petroleum products in general)

发布单位

US-ASTM

适用范围

1.1 This test method covers the determination of total sulfur in petroleum and petroleum products that are single-phase and either liquid at ambient conditions, liquifiable with moderate heat, or soluble in hydrocarbon solvents. These materials can include diesel fuel, jet fuel, kerosine, other distillate oil, naphtha, residual oil, lubricating base oil, hydraulic oil, crude oil, unleaded gasoline, M-85 and M-100.

1.2 The interlaboratory study on precision covered a variety of materials with sulfur concentrations ranging from approximately 3 mg/kg to 5.3 mass %. For a subset of these samples, with sulfur concentrations below 60 mg/kg, the repeatability standard deviation (S_r) was 1.5 mg/kg. An estimate of the limit of detection is 3 X S_r , and an estimate of the limit of quantitation 2 is 10 X S_r. However, because instrumentation covered by this test method can vary in sensitivity, the applicability of the test method at sulfur concentrations below approximately 20 mg/kg must be determined on an individual basis.

1.3 Samples containing more than 5.0 mass % sulfur can be diluted to bring the sulfur concentration of the diluted material within the scope of this test method.

1.4 Volatile samples (such as high vapor pressure gasolines or light hydrocarbons) may not meet the stated precision because of selective loss of light materials during the analysis.

1.5 A fundamental assumption in this test method is that the standard and sample matrix are well matched. Matrix mismatch can be caused by C/H ratio differences between samples and standards (see Tables 1 and 2) or by the presence of other heteroatoms (see Table 3).

1.6 The values stated in either SI units or angstrom units are to be regarded separately as standard.

1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard information, see Note 1.

ASTM D2622-2003 中可能用到的仪器设备