ASTM D4517-2004(2009)
用无焰原子吸收光谱法测量高纯度水中低量硅总量的标准试验方法

Standard Test Method for Low-Level Total Silica in High-Purity Water by Flameless Atomic Absorption Spectroscopy


ASTM D4517-2004(2009) 发布历史

Control of silica in boiler feedwater and boiler water is necessary to minimize the formation of scale-forming silicates that decrease heat transfer in the boiler. Volatilization and carryover of silica with the steam may cause hard, glassy siliceous deposits to form on turbine blades that reduce turbine efficiency.

Colloidal silica that is not removed by boiler water pretreatment processes may be solubilized in the boiler and thus contribute to the dissolved silica concentration in the boiler. Both dissolved and total silica are of interest.

1.1 This test method covers the determination of total silica in water.

1.2 This test method is applicable in the range from 25 to 250 x03BC;g/L of silica as SiO2. Higher concentrations may be determined by decreasing the aliquot volume (see Note 6). Concentration range should not be extended by dilution.

1.3 This test method determines total silica, and does not distinguish between soluble and insoluble forms.

1.4 This test method was tested on reagent water only. It is the user's responsibility to assure the validity of the test method for waters of other matrices.

1.5 This standard does not purport to address the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM D4517-2004(2009)由美国材料与试验协会 US-ASTM 发布于 2004。

ASTM D4517-2004(2009) 在中国标准分类中归属于: Z16 水环境有毒害物质分析方法。

ASTM D4517-2004(2009)的历代版本如下:

  • 2004年05月01日 ASTM D4517-04 通过无焰原子吸收光谱法测定高纯度水中低水平总二氧化硅的标准测试方法
  • 2009年10月01日 ASTM D4517-04(2009) 通过无焰原子吸收光谱法测定高纯度水中低水平总二氧化硅的标准测试方法
  • 2015年08月01日 ASTM D4517-15 通过无焰原子吸收光谱法测定高纯度水中低水平总二氧化硅的标准测试方法
  • 1985年 ASTM D4517-1985(1999) 使用无火焰原子吸收光谱法测定高纯度水中的低量硅总量的标准试验方法
  • 2004年 ASTM D4517-2004 用无焰原子吸收光谱法测量高纯度水中低量硅总量的标准试验方法
  • 2004年 ASTM D4517-2004(2009) 用无焰原子吸收光谱法测量高纯度水中低量硅总量的标准试验方法
  • 2015年 ASTM D4517-2015 使用无火焰原子吸收光谱法对高纯水进行低水平全硅测定的标准试验方法
  • 1999年06月10日 ASTM D4517-85(1999) 通过无焰原子吸收光谱法测定高纯度水中低水平总二氧化硅的标准测试方法

 

 

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标准号
ASTM D4517-2004(2009)
发布日期
2004年
实施日期
废止日期
中国标准分类号
Z16
国际标准分类号
71.060.20 (Oxides)
发布单位
US-ASTM
适用范围

Control of silica in boiler feedwater and boiler water is necessary to minimize the formation of scale-forming silicates that decrease heat transfer in the boiler. Volatilization and carryover of silica with the steam may cause hard, glassy siliceous deposits to form on turbine blades that reduce turbine efficiency.

Colloidal silica that is not removed by boiler water pretreatment processes may be solubilized in the boiler and thus contribute to the dissolved silica concentration in the boiler. Both dissolved and total silica are of interest.

1.1 This test method covers the determination of total silica in water.

1.2 This test method is applicable in the range from 25 to 250 x03BC;g/L of silica as SiO2. Higher concentrations may be determined by decreasing the aliquot volume (see Note 6). Concentration range should not be extended by dilution.

1.3 This test method determines total silica, and does not distinguish between soluble and insoluble forms.

1.4 This test method was tested on reagent water only. It is the user's responsibility to assure the validity of the test method for waters of other matrices.

1.5 This standard does not purport to address the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


ASTM D4517-2004(2009) 中可能用到的仪器设备





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