This part of GB/T 12006 specifies the method for the determination of the viscosity of dilute solutions of polyamides in certain specified solvents. Polyamide samples should be completely dissolved in the chosen solvent. Additives such as flame retardants and modifiers often affect the viscosity test. In formic acid, the viscosity will be higher, and in sulfuric acid, the viscosity will be lower. The degree of influence on polyamide compounds depends on conditions such as additives, additive levels, some other additives present and formulation. For pure polyamides or polyamides containing additives that have no effect on the viscosity test, the determination of the viscosity number provides a method for determining the molecular weight of the polymer. Pure polyamides or polyamides containing additives that have no effect on the viscosity test, the viscosity number can be switched from one solvent to another. For polyamides containing additives which affect the viscosity test, the viscosity number shall indicate the solvent used and the composition of the material. In this case, the viscosity number determination cannot be converted from one solvent to another. This method is applicable to PA46, PA6, PA66, PA69, PA610, PA612, PAll, PA12, PA6T/66, PA6I/6T, PA6T/6I/66, PA6T/61, PA6I/6T/66 named according to ISO 1874-1 Polyamides with PA MXD6, copolyamides, polyamide compounds and other polyamides that are soluble in a specified solvent under specified conditions. This method is not applicable to polyamides produced by the anionic polymerization of lactams or by cross-linking agents, which are generally insoluble in the specified solvents. The viscosity number is determined according to the specific conditions specified in this part and the general procedures specified in GB/T 1632.1-2008.
GB/T 12006.1-2009 Referenced Document
ASTM D789 Standard Test Methods for Determination of Relative Viscosity and Moisture Content of Polyamide (PA)
GB/T 1632.1-2008 Plastics.Determination of the viscosity of polymers in dilute solution using capillary viscometers.Part 1:General principles