71.080.15 芳香烃 标准查询与下载



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Determination of hydrocarbon components in crude aromatic hydrocarbons for industrial use by gas chromatography

ICS
71.080.15
CCS
G17
发布
2016-07-11
实施
2017-01-01

5.1 This test method is suitable for setting specifications, for use as an internal quality control tool, and for use in development or research work on industrial aromatic hydrocarbons and related materials. 5.2 This test method gives a broad indication of general purity and can also indicate presence of excessive moisture. It will not differentiate between products of similar boiling range. 1.1 This test method covers the distillation of industrial aromatic hydrocarbons and related materials of relatively narrow boiling ranges from 30 to 250°C. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 The following applies to all specified limits in this test method: for the purposes of determining conformance to this test method, an observed or calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29. 1.4 Warning—Mercury has been designated by EPA and many state agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for details and EPA’s website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury or mercury-containing products, or both, in your state may be prohibited by state law. 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, 6.6.1 and Section 7.

Standard Test Method for Distillation of Industrial Aromatic Hydrocarbons and Related Materials

ICS
71.080.15
CCS
发布
2016-06-01
实施

5.1 This test method is suitable for setting specifications, for use as an internal quality control tool, and for use in development or research work on industrial aromatic hydrocarbons and related materials. This test method gives an indication of residual acidity and is a measure of the quality of the finished product. It is an indication of the tendency of the product to corrode equipment. 1.1 This test method is intended for the detection of acidity of benzene, toluene, xylenes, solvent naphthas, and similar industrial aromatic hydrocarbons. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements see Section 9.

Standard Test Method for Acidity of Benzene, Toluene, Xylenes, Solvent Naphthas, and Similar Industrial Aromatic Hydrocarbons

ICS
71.080.15
CCS
发布
2016-06-01
实施

Standard Test Method for Analysis of Styrene by Capillary Gas Chromatography

ICS
71.080.15
CCS
发布
2016-06-01
实施

5.1 This test method can be used for determining polymer concentrations in styrene monomer. 5.2 This test method will not detect dimers and trimers. 5.3 This test method can be used for plant control and for specification analysis. 1.1 These test methods cover the determination of the polymer content of styrene monomer. It should be noted, however, that dimers and trimers are not measured by these test methods. 1.2 Test Method A, which is based on the use of a spectrophotometer or photometer, is intended for the quantitative determination of the polymer content of styrene monomer in concentrations up to 15 mg/kg. Samples containing more than 15 mg/kg of polymer must be suitably diluted before measurement. 1.3 Test Method B is a rapid visual procedure that is intended for the approximate evaluation of polymer to a maximum concentration of 1.0 mass %. Samples having a polymer content of 1.0 mass8201;% or greater should be suitably diluted prior to measurement. 1.4 In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29. 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 9.

Standard Test Methods for Polymer Content of Styrene Monomer

ICS
71.080.15
CCS
发布
2016-06-01
实施

5.1 This test method may be used as a criteria for determining the purity of benzene. The closer the solidification point reaches that of pure benzene, the purer the sample. 1.1 This test method covers the determination of the solidification point of benzene. 1.2 In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 7.

Standard Test Method for Solidification Point of Benzene

ICS
71.080.15
CCS
发布
2016-06-01
实施

5.1 This test method provides for the precise measurement of the chlorine content of aromatics with minimal sample preparation and analyst involvement. The typical time for each analysis is five or ten minutes. 5.2 Knowledge of the chlorine content of aromatics is important for process control as well as the prediction and control of operational problems such as unit corrosion and catalyst poisoning, and in the blending of products to commodity specifications. 5.3 Various federal, state, and local agencies regulate the chlorine content of some petroleum products, including aromatics. Unbiased and precise determination of chlorine in aromatics is critical to compliance with regulatory standards. 5.4 When the elemental composition of the samples differ significantly from the calibration standards used to prepare the calibration curve, the cautions and recommendation in Section 6 should be carefully observed. 1.1 This test method covers the determination of chlorine by monochromatic, wavelength-dispersive X-ray fluorescence (MWDXRF) spectrometry in aromatic hydrocarbons, their derivatives, and related chemicals. 1.2 This test method is applicable to samples with chlorine concentrations from 0.66 mg/kg to 10.07 mg/kg. Higher chlorine concentrations can be determined by quantitatively diluting the sample with a suitable solvent. In an interlaboratory study, the limit of detection was determined to be 0.18 mg/kg. 1.3 In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29. 1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard information, see Section 9.

Standard Test Method for Chlorine in Aromatics by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry

ICS
71.080.15
CCS
发布
2016
实施

1.1 This specification covers a grade of o-xylene identified as ortho-Xylene 980. 1.2 The following applies to all specified limits in this specification: for purposes of determining conformance with this specification, an observed value or a calculated value shall be rounded off to the nearest unit in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 Consult current OSHA regulations and supplier’s Safety Data Sheets, and local regulations for all materials used in this specification.

Standard Specification for O-Xylene 980

ICS
71.080.15
CCS
发布
2016
实施

1.1 This specification covers toluene for toluene diisocyanate (TDI) feedstock. 1.2 The following applies to all specified limits in this specification: for purposes of determining conformance with this specification, an observed value or a calculated value shall be rounded off to the nearest unit in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29. 1.3 Consult OSHA regulations and supplier’s Safety Data Sheets for all materials used in this specification. 1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.

Standard Specification for Toluene for Toluene Diisocyanate (TDI) Feedstock

ICS
71.080.15
CCS
发布
2016
实施

1.1 This specification covers nitration grade xylene. 1.2 The following applies to all specified limits in this standard: for purposes of determining conformance with this standard, an observed value or a calculated value shall be round off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the round-off method of Practice E29. 1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only. 1.4 Consult OSHA regulations, supplier’s Safety Data Sheets, and local regulations for all materials used in this specification.

Standard Specification for Nitration Grade Xylene

ICS
71.080.15
CCS
发布
2016
实施

1.1 This specification covers cumene (isopropylbenzene). 1.2 The following applies to all specified limits in this specification: for purposes of determining conformance with this specification, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29. 1.3 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 Consult current OSHA Regulations and Supplier’s Safety Data Sheets, and local regulations for all materials used in this specification.

Standard Specification for Cumene (Isopropylbenzene)

ICS
71.080.15
CCS
发布
2016
实施

3.1 This practice is issued to provide information useful in establishing sampling and handling procedures. It is expected that this information will only be utilized in conjunction with an existing health and safety program and consultation with an appropriate SDS. The information provided cannot be used as a substitute for expert safety and medical advice as provided in an appropriate SDS, but rather as a supplement to such advice. 1.1 This practice covers procedures for sampling and handling phenol, cresols and cresylic acid in solid and liquid forms, including liquids at elevated temperatures, in a safe manner that represents and preserves quality. In general, this practice also applies to xylenols, and some other alkylated phenolic materials; however, specific information regarding these materials should be sought and used if available. 1.2 Any person sampling or handling these products should consult the applicable Safety Data Sheet (SDS) for specific first aid instructions and information on the proper equipment to have available for use in the event of personal contact or exposure. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 3, 4, 5, 6, 7, 8 and an appropriate SDS.

Standard Practice for Sampling and Handling Phenol, Cresols, and Cresylic Acid

ICS
71.080.15
CCS
发布
2016
实施

1.1 This specification covers xylenes for p-xylene feedstock. These xylenes typically are extracted from reformate. 1.2 The following applies to all specified limits in this specification: for purposes of determining conformance with this specification, an observed value or calculated value shall be rounded off “to the nearest unit” in the last right hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29. 1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only. 1.4 Consult current OSHA regulations, suppliers’ Safety Data Sheets (SDS), and local regulations for all materials used in this specification.

Standard Specification for Xylenes for p-Xylene Feedstock

ICS
71.080.15
CCS
发布
2016
实施

4.1 This test method is useful in determining phenol in the range from 5 to 50 mg/kg in commercially available cumene or AMS. 4.2 Phenol will inhibit certain reactions involving cumene or AMS. 1.1 This test method covers the determination of phenol in refined cumene (isopropylbenzene) or AMS (α–methylstyrene). 1.2 This test method has been found applicable in the range from 5 to 50 mg/kg of phenol in refined cumene (isopropylbenzene) or AMS (α–methylstyrene). 1.3 In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29. 1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 7.

Standard Test Method for Phenol Content of Cumene (Isopropylbenzene) or AMS (α&x2013;Methylstyrene)

ICS
71.080.15
CCS
发布
2016
实施

1.1 This specification covers benzene for use with zeolite based catalysts. 1.2 The following applies to all specified limits in this specification: for purposes of determining conformance with this specification, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29. 1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.4 Consult current OSHA regulations, supplier’s Safety Data Sheets, and local regulations for all materials used in this specification.

Standard Specification for Benzene for Use with Zeolite Based Catalysts

ICS
71.080.15
CCS
发布
2016
实施

本标准规定了焦炉煤气中硫化氢含量的气相色谱测定的原理、仪器和材料、采样、分析步骤、结果计算、精密度和安全注意事项。 本标准适用于焦炉煤气中硫化氢含量的测定。

Coke oven gas.Determination of the hydrogen sulfide content.Gas chromatography

ICS
71.080.15
CCS
G17
发布
2015-07-14
实施
2016-01-01

本标准规定了测定焦炉煤气中氰化氢含量的试剂、仪器设备、取样、分析步骤和结果计算。 本标准适用于高温炼焦所得的焦炉煤气中氰化氢含量的测定,测定范围:0.1g/m~2.0g/m。

Coke oven gas.Determination of the hydrogen cyanide content.Silver nitrate titration method

ICS
71.080.15
CCS
G17
发布
2015-07-14
实施
2016-01-01

1.1 This specification covers ethylbenzene. 1.2 Consult current OSHA regulations, supplier’s Safety Data Sheet for all materials, and local regulations used in this specification. 1.3 The following applies to all specified limits in this specification for purposes of determining conformance with this specification, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.

Standard Specification for Ethylbenzene

ICS
71.080.15
CCS
发布
2015-06-01
实施

3.1 This practice is issued to provide information useful in establishing sampling procedures. It is expected that this information will only be utilized in conjunction with an existing health and safety program and consultation with the appropriate SDS. The information provided herein cannot be used as a substitute for expert safety and medical advice, but rather as a supplement to such advice. 1.1 This practice covers procedures for sampling and handling naphthalene, maleic anhydride, and phthalic anhydride in various solid forms, and as liquids at elevated temperatures in a safe manner that represents and preserves quality. 1.2 Any person sampling or handling these products should consult the applicable Safety Data Sheet (SDS) for specific first aid instructions and information on the proper equipment to have available for use in the event of personal contact or exposure. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 3, 4, 5, 6, and 7 and an appropriate SDS.

Standard Practice for Sampling and Handling Naphthalene, Maleic Anhydride, and Phthalic Anhydride

ICS
71.080.15
CCS
发布
2015
实施

5.1 Determining the type and amount of hydrocarbon impurities remaining from the manufacture of toluene, mixed xylenes, p-xylene, o-xylene, ethylbenzene, benzene, and styrene used as chemical intermediates and solvents is often required. This test method is suitable for setting specifications and for use as an internal quality control tool where these products are produced or are used. Typical impurities are: alkanes containing 1 to 10 carbons atoms, benzene, toluene, ethylbenzene (EB), xylenes, and aromatic hydrocarbons containing nine carbon atoms or more. 5.2 This method may not detect all components and there may be unknown components that would be assigned inappropriate response factors and thus, the results may not be absolute. 1.1 This test method covers the determination of total nonaromatic hydrocarbons and monocyclic aromatic hydrocarbons in benzene, toluene, ethylbenzene, p-xylene, o-xylene, styrene and mixed xylenes by gas chromatography. The purity of benzene, toluene, ethylbenzene, p-xylene, o-xylene, styrene and mixed xylenes is also calculated. Similar test methods, using the internal standard calibration technique and the external standard calibration technique, are Test Methods D2360, D3797, D4492, D5060, D5135, D5917, and D6563 respectively. 1.2 A small amount of benzene in toluene, ethylbenzene, p-xylene, o-xylene, styrene and mixed xylenes may not be distinguished from the non-aromatics and the concentrations are determined as a composite (see 6.1). 1.3 The limit of detection (LOD) is 0.0002 wt % and limit of quantitation (LOQ) is 0.0006 wt % for impurities in toluene, mixed xylenes, p-xylene, o-xylene, ethylbenzene, benzene, and styrene. 1.4 In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29. 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6

Standard Test Method for Trace Impurities in Monocyclic Aromatic Hydrocarbons by Gas Chromatography and Effective Carbon Number

ICS
71.080.15
CCS
发布
2015
实施



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