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The principle of the method is grinding of the laboratory sample, with or without preliminary breaking, crushing, grinding or drying, division of the sample by suitable means, taking care that the test sample thus obtained, from which the test portion(s) will be taken, truly represents the totality of the laboratory sample.
Oilseed residues; preparation of test samples
Specifies a method for the determination of hexane content after extraction with hydrocarbon-based solvents. Describes the principle, the reagents and materials, the apparatus, the sampling, the test procedure, the expression of results, and the contents of the test report.
Oilseed residues; determination of free residual hexane
Fat is extracted in accordance with BS 4289:Part 4, dissolved in hot ethanol and titrated with aqueous sodium or potassium hydroxide.
Method for the analysis of oilseeds - Determination of acidity of fat
The method consists in dissolving in a mixture of diethyl ether and ethanol of the oil extracted for the determination of the "oil contend" of the seeds (see ISO 659), and then titrating of the free fatty acids present using an ethanolic potassium hydroxide solution. It is not applicable to cotton seeds with adherent cotton linters, or to palm or olive fruits.
Oilseeds; determination of acidity of oils
For each species to be tested, preparation of samples of different moisture content, determination of their moisture contents by a reference method and measurement with the meter to be checked.
Methods for analysis of oilseeds - Check of the calibration of moisture meters
Incineration of product, ground if necessary, at 550 15C to constant mass. Apparatus, procedure, expression of results, test report. Not applicable to purposes subject to the Fertilisers and Feeding Stuffs Regulations 1973 or to the Fertilisers and Feeding Stuffs (Amendment) Regulations 1976.
Methods for analysis of oilseed residues - Determination of total ash
Treatment of total ash with 3N hydrochloric acid solution and incineration of insoluble residue. Reagents, apparatus, procedure, expression of results, test report. Not applicable to purposes subject to the Fertilisers and Feeding Stuffs Regulations 1973 or to the Fertilisers and Feeding Stuffs (Amendment) Regulations 1976.
Methods for analysis of oilseed residues. Determination of ash insoluble in hydrochloric acid
Extraction of product, ground if necessary, with diethyl ether. Reagents, apparatus, procedure, expression of results, test report. Not applicable to purposes subject to the Fertilisers and Feeding Stuffs Regulations 1973 or to the Fertilisers and Feeding Stuffs (Amendment) Regulations 1976.
Methods for analysis of oilseed residues - Determination of diethyl ether extract
Oven-drying of product, ground if necessary, at 103C to constant mass. Apparatus, procedure, expression of results, test report. Not applicable to purposes subject to the Fertilisers and Feeding Stuffs Regulations 1973 or to the Fertilisers and Feeding Stuffs (Amendment) Regulations 1976.
Methods for analysis of oilseed residues - Determination of moisture and volatile matter content
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