ASTM D5441-1998(2013)
采用气相色谱法分析甲基特丁基乙醚(MTBE)的标准试验方法
Standard Test Method for Analysis of Methyl Tert-Butyl Ether (MTBE) by Gas Chromatography
ASTM D5441-1998(2013) 中，可能用到以下仪器设备
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- 标准号
- ASTM D5441-1998(2013)
- 发布日期
- 1998年
- 实施日期
- 废止日期
- 无
- 国际标准分类号
- 71.080.60 (Alcohols. Ethers)
- 发布单位
- US-ASTM
- 适用范围
5.1x00a0;The presence of impurities in MTBE product can have a deleterious effect upon the value of MTBE as a gasoline additive. Oxygenate and olefin contents are of primary concern. This test method provides a knowledge of the composition of MTBE product. This is useful in the evaluation of process operations control, in the valuation of the product, and for regulatory purposes.
5.2x00a0;Open tubular column gas chromatography with a flame ionization detector, used by the test method, is a technique that is sensitive to the contaminants commonly found in MTBE, and a technique that is widely used.
1.1x00a0;This test method covers the determination of the purity of methyl tert-butyl ether (MTBE) by gas chromatography. It also provides a procedure to measure impurities in MTBE such as C4 to C12 olefins, methyl, isopropyl and tert-butyl alcohols, methyl sec-butyl and methyl tert-amyl ethers, acetone, and methyl ethyl ketone. Impurities are determined to a minimum concentration of 0.02 mass %.
1.3x00a0;Water cannot be determined by this test method and must be measured by a procedure such as Test Method D1364 and the result used to normalize the chromatographic values.
1.4x00a0;A majority of the impurities in MTBE is resolved by the test method, however, some co-elution is encountered.
1.5x00a0;This test method is inappropriate for impurities that boil at temperatures higher than 180x00b0;C or for impurities that cause poor or no response in a flame ionization detector, such as water.
1.6x00a0;The values stated in SI (metric) units of measurement are preferred and used throughout the standard. Alternate units, in common usage, are also provided to improve clarity and aid the user of this test method.
1.7x00a0;This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to consult and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.