71.040.50 物理化学分析方法 标准查询与下载



共找到 754 条与 物理化学分析方法 相关的标准,共 51

Microbeam analysis-Electron probe microanalysis-Guidelines for determining the carbon content of steels using a calibration curve method

ICS
71.040.50
CCS
发布
20210823
实施
20210823

1.1 This reference test method covers an experimental procedure for checking experimental technique and instrumentation. If followed, this reference test method will provide repeatable potentiodynamic anodic polarization measurements that will reproduce data determined by others at other times and in other laboratories provided all laboratories are testing reference samples from the same lot of Type 430 stainless steel. 1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Reference Test Method for Making Potentiodynamic Anodic Polarization Measurements

ICS
71.040.50
CCS
发布
2021-08-01
实施

Liquid chromatography at critical conditions (LCCC) - Chemical heterogeneity of polyethylene oxides (ISO/TS 23973:2020)

ICS
71.040.50
CCS
发布
2021-08-00
实施

This document describes procedures for measuring average grain size derived from a two-dimensional polished cross-section using electron backscatter diffraction (EBSD). This requires the measurement of orientation, misorientation and pattern quality factor as a function of positi

Microbeam analysis - Electron backscatter diffraction - Measurement of average grain size (ISO 13067:2020)

ICS
71.040.50
CCS
发布
2021-08-00
实施

1.1 This test method covers a high performance liquid chromatographic test method for the determination of monoaromatic and di-aromatic hydrocarbon contents in aviation kerosenes and petroleum distillates boiling in the range from 50 °C to 300 °C, such as Jet A or Jet A-1 fuels. The total aromatic content is calculated from the sum of the individual aromatic hydrocarbon-types. NOTE 1—Samples with a final boiling point greater than 300 °C that contain tri-aromatic and higher polycyclic aromatic compounds are not determined by this test method and should be analyzed by Test Method D6591 or other suitable equivalent test methods. 1.2 This test method is applicable to distillates containing from 0.8 % to 44.0 % by mass mono-aromatic hydrocarbons, 0.23 % to 6.20 % by mass di-aromatic hydrocarbons, and 0.7 % to 50 % by mass total aromatics. Although this method generates results in m/m, results may also be quoted in v/v. 1.3 The precision of this test method has been established for kerosene boiling range distillates containing from 0.40 % to 44.0 % by mass mono-aromatic hydrocarbons, 0.02 % to 6.20 % by mass di-aromatic hydrocarbons, and 0.40 % to 50.0 % by mass total aromatics. If results are quoted in volume, the precision is 0.3 % to 41.4 % by volume mono-aromatics, 0.01 % to 5.00 % by volume di-aromatics, and 0.30 % to 46.3 % by volume total aromatics. As calculated by IP 367-1. 1.4 Compounds containing sulfur, nitrogen, and oxygen are possible interferents. Mono-alkenes do not interfere, but conjugated diand poly-alkenes, if present, are possible interferents. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. 1 This test method is under the jurisdiction of ASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of Subcommittee D02.04.0C on Liquid Chromatography. The technically equivalent standard as referenced is under the jurisdiction of the Energy Institute Subcommittee SC-G-2. Current edition approved July 15, 2021. Published September 2021. Originally approved in 1999. Last previous edition approved in 2019 as D6379 – 11 (2019). DOI: 10.1520/D6379-21E01. 2 This test method has been developed through the cooperative effort between ASTM and the Energy Institute, London. ASTM and IP standards were approved by ASTM and EI technical committees as being technically equivalent but that does not imply both standards are identical. *A Summary of Changes section appears at the end of this standard Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. 1 2. Referenced Documents

Standard Test Method for Determination of Aromatic Hydrocarbon Types in Aviation Fuels and Petroleum Distillates—High Performance Liquid Chromatography Method with Refractive Index Detection

ICS
71.040.50
CCS
发布
2021-07-15
实施

Standard Test Method for Determination of Aromatic Hydrocarbon Types in Aviation Fuels and Petroleum Distillates—High Performance Liquid Chromatography Method with Refractive Index Detection

ICS
71.040.50
CCS
发布
2021-07-15
实施

建立碳化硼-碳化硅的电感耦合等离子发射光谱法(ICP-OES)电感耦合等离子体质谱(ICP-MS)法的测试标准。 其主要内容包括: 1试样的制备。 2.测试方法的确定:包括试剂和材料、标准溶液的配制、样品处理、仪器条件、测试过程、测试结果计算。 3.检测方法的精密度。

Determination of trace elements in boron carbide–silicon carbide pellets by Inductively coupled plasma optical emission spectrometry

ICS
71.040.50
CCS
M732
发布
2021-06-14
实施
2021-08-17

1.1 This test method covers a procedure for determination of the relative crystallinity of zeolite ZSM-5 using selected peaks from the X-ray diffraction pattern of the zeolite. 1.2 The test method provides a number that is the ratio of intensity of a portion of the XRD pattern of the sample ZSM-5 to intensity of the corresponding portion of the pattern of a reference ZSM-5. The intensity ratio, expressed as a percentage, is then labeled percent XRD relative crystallinity/ ZSM-5. This type of comparison is commonly used in zeolite technology and is often referred to as percent crystallinity. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Test Method for Determination of Relative Crystallinity of Zeolite ZSM-5 by X-Ray Diffraction

ICS
71.040.50
CCS
发布
2021-06-01
实施

1.1 This standard outlines the methods that can be used to deconvolve, at least partially, the spectral bandpass differences of raw spectral data acquired by abridged spectrophotometry. Such differences are introduced because the spectral passband must be of significant bandwidth to allow sufficient energy to reach the detector. On the other hand, the spectral data that should be reported is that of a virtual 1-nm bandwidth spectrum in order to be useful in the CIE method of tristimulus integration which involves 1-nm summation. 1.2 The standard establishes practices for whether, when, and how a bandpass rectification should be made to any reflectance or transmittance spectrum acquired by abridged spectrophotometry. 1.3 It is applicable where the shape of the passband is triangular and the bandwidth is equal to the measurement interval between passbands. Information is provided in Section 7 for users when that condition is not satisfactorily met. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Practice for Rectification of Spectrophotometric Bandpass Differences

ICS
71.040.50
CCS
发布
2021-06-01
实施

1.1?This test method provides necessary information to determine the total amount of moisture (physisorbed and chemisorbed water molecules) in a plutonium dioxide (PuO2) sample using a combination of thermogravimetric and mass spectrometric analyses. This test method is useful w

Standard Test Method for Moisture Analysis of Plutonium Dioxide (PuO2) by Thermogravimetric Mass Spectrometry (TGA-MS)

ICS
71.040.50
CCS
发布
2021-06-01
实施

What is ISO 23420 about?    ISO 23420 discusses microbeam Analysis. ISO 23420 specifies a determination procedure of energy resolution in the scanning transmission electron microscope, or the transmission electron microscope equipped with the electron energy loss (EEL) spectrometer.   Note: ISO 23420 is applicable to both in-column type EEL spectrometer and post-column type EEL spectrometer. These EEL signal detecting systems are applicable to a parallel detecting system and a serial detecting system.  Who is ISO 23420 for?   ISO 23420

Microbeam analysis. Analytical electron microscopy. Method for the determination of energy resolution for electron energy loss spectrum analysis

ICS
71.040.50
CCS
发布
2021-05-31
实施
2021-05-31

1.1 This practice provides direction for establishing and controlling spark atomic emission spectrochemical analytical curves. The generation of analytical curves and their control are considered as separate though interrelated operations. This practice is applicable to spark atomic emission spectrometers. NOTE 1—X-ray fluorescence spectrometric applications are no longer covered by this practice. See Guides E1361 and E1621 for discussion of this technique. 1.1.1 Since software programs are readily available to compute multiple linear regressions that can be used to generate analytical curves and since most instruments include this feature, this practice does not address this procedure. However, some recommendations are given to evaluate the equations that are generated. 1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Practice for Establishing and Controlling Spark Atomic Emission Spectrochemical Analytical Curves

ICS
71.040.50
CCS
发布
2021-05-15
实施

本标准适用于碳化硼基体的核电堆芯材料中4种无机阴离子(F-、Cl-、Br-、I-)的测定。规定了离子色谱(IC)法测定碳化硼-碳化硅芯块中无机阴离子(F-、Cl-、Br-、I-)含量的原理、试剂或材料、仪器和设备、分析步骤、精密度等内容。

Determination of Inorganic Anions(F-、Cl-、Br-、I-) in boron carbide – silicon carbide pellets By Ion Chromatography

ICS
71.040.50
CCS
M745
发布
2021-05-14
实施
2021-08-24

本文件规定了玻璃、陶瓷包装容器在食品模拟物中浸泡后铅、镉、砷、锑、锰迁移量测定的电感耦合等离子体发射光谱(ICP-OES)法。 本文件适用于玻璃、陶瓷包装容器中铅、镉、砷、锑、锰迁移量的测定。 本文件适用于盛装食品、酒、饮料、饮用水等各种玻璃、陶瓷包装容器。其他非玻璃、陶瓷包装容器可参照采用。

Packaging glass containers — Determination of the release of lead, cadmium, arsenic, antimony and manganese — Inductively Coupled Plasma Optical Emission Spectrometer (ICP-OES) method

ICS
71.040.50
CCS
M745
发布
2021-05-10
实施
2021-05-11

This document specifies a determination procedure of energy resolution in the scanning transmission electron microscope or the transmission electron microscope equipped with the electron energy loss (EEL) spectrometer. This document is applicable to both in-column type EEL spectrometer and post-column type EEL spectrometer. These EEL signal detecting systems are applicable to a parallel detecting system and a serial detecting system.

Microbeam analysis — Analytical electron microscopy — Method for the determination of energy resolution for electron energy loss spectrum analysis

ICS
71.040.50
CCS
发布
2021-04-23
实施

Microbeam analysis. Electron probe microanalysis. Quantitative analysis of Mn dendritic segregation in continuously cast steel product

ICS
71.040.50
CCS
发布
2021-04-20
实施
2021-04-20

1.1 These practices provide general recommendations covering the various techniques commonly used in obtaining internal reflection spectra.2,3 Discussion is limited to the infrared region of the electromagnetic spectrum and includes a summary of fundamental theory, a description of parameters that determine the results obtained, instrumentation most widely used, practical guidelines for sampling and obtaining useful spectra, and interpretation features specific for internal reflection. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Practices for Internal Reflection Spectroscopy

ICS
71.040.50
CCS
发布
2021-04-01
实施

1.1?This test method covers the use of gas chromatography and vacuum ultraviolet absorption spectroscopy (GC-VUV) for the determination of individual compounds and compound classes by percent mass or percent volume with a final boiling point as defined by Test Method D86 up to 2

Standard Test Method for Detailed Hydrocarbon Analysis by High Resolution Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy (GC-VUV)

ICS
71.040.50
CCS
发布
2021-04-01
实施

1.1 This practice covers the installation and maintenance of fused silica capillary columns in gas chromatographs that are already retrofitted for their use. This practice excludes information on: 1.1.1 Injection techniques. 1.1.2 Column selection. 1.1.3 Data acquisition. 1.1.4 System troubleshooting and maintenance. 1.2 For additional information on gas chromatography, please refer to Practice E260. For specific precautions, see 7.2.2.2(1), 7.2.2.2(2), 7.2.7, and 7.2.7.2. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific safety information, see Section 6, 7.2.2.2(1), 7.2.2.2(2), 7.2.7, and 7.2.7.2.2 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs

ICS
71.040.50
CCS
发布
2021-04-01
实施

1.1 This practice covers the spectral range from 4000 cm−1 to 50 cm−1 and includes techniques that are useful for qualitative analysis of liquid-, solid-, and vapor-phase samples by infrared spectrometric techniques for which the amount of sample available for analysis is not a limiting factor. These techniques are often also useful for recording spectra at frequencies higher than 4000 cm–1 , in the near-infrared region. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautions are given in 6.5.1. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Practice for General Techniques for Obtaining Infrared Spectra for Qualitative Analysis

ICS
71.040.50
CCS
发布
2021-04-01
实施



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