Z13 固体废弃物、土壤及其他环境要素采样方法 标准查询与下载

EN 15267-4:2017 空气质量-自动测量系统的质量保证-第4部分:定期测量固定源排放量自动测量系统的性能标准和试验程序

This European Standard specifies the general performance criteria and test procedures for portable automated measuring systems (P-AMS) used for periodic measurements of stationary source emissions. It applies to the performance testing of P-AMS based on measurement techniques specified by the standard reference method (SRM) or an alternative method (AM). Performance testing is based on the general performance criteria and test procedures specified in this European Standard and on the specific requirements specified for the SRM or AM. This includes testing of the applicability and correct implementation of the QA/QC procedures specified for the SRM or AM. This European Standard supports the requirements of particular EU Directives.

Air quality - Certification of automated measuring systems - Part 4: Performance criteria and test procedures for automated measuring systems for periodic measurements of emissions from stationary sources

PD CEN/TS 17021:2017 固定源排放 用仪器技术测定二氧化硫的质量浓度

This Technical Specification describes a method for sampling and determining the concentration of gaseous sulphur dioxide (SO2) emissions from stacks. This method is based on instrumental techniques. It is applicable to both periodic measurements and the calibration of automated measuring systems permanently installed on stacks, for regulatory or other purposes.

Stationary source emissions - Determination of the mass concentration of sulphur dioxide by instrumental techniques

ASTM D5057-17 废弃物的堆积密度和筛选表观比重的标准试验方法

5.1 This test method is intended for use by those in the waste management industries for the determination of apparent specific gravity and bulk density of waste. 5.2 The apparent specific gravity and bulk density determined by this test method can be used for the conversion of measured volumes to weights. 5.3 The apparent specific gravity and bulk density, when correlated with other properties, can be used to indicate the character of the waste. 1.1 This test method covers the determination of apparent specific gravity and bulk density in a waste sample. For the purpose of this test method, the property to be measured is classified into three groups based on material type: 1.1.1 Group A—Free-flowing liquids; apparent specific gravity (ASG), 1.1.2 Group B—Granules, powders, and water-reactive liquids, solids, or sludges; bulk density (BD), and 1.1.3 Group C—Bulk solids (such as gravel, paper, or wood, etc.); apparent specific gravity (ASG). 1.2 This test method is designed and intended as a screening test to complement the more sophisticated quantitative analytical techniques that may be used to determine specific gravity. This test method offers to the user the option and the ability to screen waste for apparent specific gravity or bulk density when the more sophisticated techniques are not available and the total waste composition is unknown. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Test Method for Screening Apparent Specific Gravity and Bulk Density of Waste

ASTM D5198-17 固体废弃物的硝酸处理的标准实施规程

5.1 A knowledge of the inorganic composition of a waste is often required for the selection of appropriate waste disposal practices. Solid waste may exist in a variety of forms and contain a range of organic and inorganic constituents. This practice describes a digestion procedure which dissolves many of the toxic inorganic constituents and produces a solution suitable for determination of total recoverable contents by such techniques as atomic absorption spectroscopy, atomic emission spectroscopy, and so forth. The relatively large sample size aids representative sampling of heterogenous wastes. The relatively small dilution factor allows lower detection limits than most other sample digestion methods. Volatile metals, such as lead and mercury, are not lost during this digestion procedure, however organo-lead and organo-mercury may not be completely digested. Hydride-forming elements, such as arsenic and selenium, may be partially lost. Samples with total metal contents greater than 58201;% may give low results. The analyst is responsible for determining whether this practice is applicable to the solid waste being tested. 1.1 This practice describes the partial digestion of solid waste using nitric acid for the subsequent determination of the total recoverable content of inorganic constituents. 1.2 This practice is to be used when the concentrations of total recoverable elements are to be determined from a waste sample. Total recoverable elements are often not equivalent to total elemental content, because of the solubility of the speciated forms of the element in the sample matrix. Recovery from refractory sample matrices, such as soils, is usually significantly less than total concentrations of the elements present. Note 1: This practice has been used successfully for oily sludges and a municipal digested sludge standard [Environmental Protection Agency (EPA) Sample No. 397]. The practice may be applicable to some elements not listed above, such as arsenic, barium, selenium, cobalt, magnesium, and calcium. Refractory elements such as silicon, silver, and titanium, as well as organo-mercury, are not solubilized by this practice. 1.3 This practice has been divided into two methods, A and B, with Method A utilizing an electric hot plate and Method B utilizing an electric digestion block. 1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Standard Practice for Nitric Acid Digestion of Solid Waste

EN 15308:2016 废弃物的特性-用带电子俘获或质谱检测的气相色谱法测定固体废弃物中选择的多氯化联二苯(PCB)

This European Standard specifies a method for quantitative determination of seven polychlorinated biphenyl congeners (PCB-28, PCB-52, PCB-101, PCB-118, PCB-138, PCB-153 and PCB-180) in solid waste using high-resolution gas chromatography with electron capture or mass spectrometric detection. The basic content of this standard is identical to that of the Horizontal PCB-standard and is therefore also applicable to soil, sludge and treated bio-waste. The detection and the quantification limits in this method are dependent on sample intake, the level of interferences as well as instrumental limitations. Under the conditions specified in this standard, minimum amounts of individual PCB congeners equal or above 0,01 mg/kg dry matter can typically be determined with no interferences present. NOTE For the analysis of PCB in insulating liquids, petroleum products, used oils and aqueous samples is referred to EN 61619, EN 12766-1 and EN ISO 6468 respectively. The method may be applied to the analysis of other PCB congeners not specified in the scope, but its suitability should be proven by proper in-house validation experiments.

Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection

EN ISO 14644-14:2016 洁净室和相关受控环境第14部分:由尘埃粒子浓度使用设备的适宜性评价(ISO 14644-14:2016)

Dieser Teil von ISO 14644 legt eine Methodik zur Bewertung der Reinraumtauglichkeit von Geräten (z. B. Maschinen, Messgeräte, Prozessausrüstung, Komponenten und Werkzeuge) für die Anwendung in Reinräumen und zugehörigen kontrollierten Bereichen in Bezug auf die luftgetragene Partikelreinheit nach den Festlegungen in ISO 14644-1 fest. Der Partikelgrößenbereich reicht von 0,1 µm bis gleich oder größer als 5 µm (in ISO 14644-1 angegeben). ANMERKUNG Sofern die zuständigen Behörden ergänzende Richtlinien oder Einschränkungen vorgeben, können geeignete Anpassungen der Methodik zur Bewertung erforderlich sein. Die folgenden Aspekte sind nicht durch diesen Teil von ISO 14644 abgedeckt: Bewertung der Tauglichkeit in Bezug auf die Biokontamination; Prüfung zur Tauglichkeit von Dekontaminationsmitteln und -techniken; Reinigungsfähigkeit der Geräte und Materialien; Anforderungen an die konstruktive Auslegung von Geräten und die Auswahl von Materialien; physikalische Materialeigenschaften (z. B. elektrostatische, thermische Eigenschaften); Optimierung der Geräteleistung für spezifische Prozessanwendungen; Auswahl und Anwendung statistischer Verfahren für die Prüfung; Protokolle und Anforderungen hinsichtlich regionaler Sicherheitsvorschriften.

Cleanrooms and associated controlled environments - Part 14: Assessment of suitability for use of equipment by airborne particle concentration

HJ 782-2016 固体废物 有机物的提取 加压流体萃取法

本标准规定了提取固态固体废物中有机物的加压流体萃取法。 本标准适用于固态固体废物中有机磷农药、有机氯农药、氯代除草剂、多环芳烃、邻苯二甲酸酯、多氯联苯等半挥发性有机物和不挥发性有机物的提取，详见附录Ａ。若通过验证，本标准也可适用于固态固体废物中其他有机物的提取。

Waste solid-- Extraction of organic compounds -- Pressurized fluid extraction（PFE）

DIN 19529:2015 固体材料的浸出.液固比为21/kg无机与有机物质浸出性能的检验用批量试验

Leaching of solid materials - Batch test for the examination of the leaching behaviour of inorganic and organic substances at a liquid to solid ratio of 2 l/kg

HJ 765-2015 固体废物 有机物的提取 微波萃取法

本标准规定了提取固体废物中有机物的微波萃取法。 本标准适用于固体废物中多环芳烃、酞酸酯、有机氯农药、有机磷农药以及多氯联苯等有机物的提取。

Waste solid-Distilling of organic compound - Microwave extraction

DIN EN ISO 11268-3:2015 土质.污染物对蚯蚓的影响.第3部分:野外影响的测定指南(ISO 11268-3-2014);德文版本EN ISO 11268-3-2015

Soil quality - Effects of pollutants on earthworms - Part 3: Guidance on the determination of effects in field situations (ISO 11268-3:2014); German version EN ISO 11268-3:2015

DIN EN ISO 11268-2:2015 土质. 污染物对蚯蚓的影响. 第2部分:赤子爱胜蚓/安德爱胜蚓繁殖影响的测定 (ISO 11268-2-2012);德文版本EN ISO 11268-2-2015

Soil quality - Effects of pollutants on earthworms - Part 2: Determination of effects on reproduction of Eisenia fetida/Eisenia andrei (ISO 11268-2:2012); German version EN ISO 11268-2:2015

NF X31-252-1*NF EN ISO 11268-1:2015 土质 - 污染物对蚯蚓的影响 - 第1部分: 测定对赤子爱胜蚓/安德爱胜蚓的剧烈毒性

Soil quality - Effects of pollutants on earthworms - Part 1 : determination of acute toxicity to Eisenia fetida/Eisenia andrei

DIN ISO 18589-2:2015 环境辐射的测量.土壤.第2部分:样品的取样策略、取样和预处理的选择指南(ISO 18589-2-2015)

Measurement of radioactivity in the environment - Soil - Part 2: Guidance for the selection of the sampling strategy, sampling and pre-treatment of samples (ISO 18589-2:2015)

BS EN 15002:2015 废物的表征 从实验室样品中制备测试部分

Characterization of waste. Preparation of test portions from the laboratory sample

EN 15002:2015 废弃物的表征.试验室样本的试验部分准备

This European Standard is applicable for the preparation of representative test portions from the laboratory sample that has been taken according to the sampling plan (EN 14899), prior to physical and/or chemical analysis (e. g. preparation of eluates, extractions, digestion and/or analytical determinations) of solid (including monolithic material) and liquid samples and sludge. It is also applicable for the preparation of test portions from digests and eluates for the subsequent analyses. This European Standard is intended to find the correct sequence of operations and treatments to be applied to the laboratory sample in order to obtain suitable test portions in compliance with the specific requirements defined in the corresponding analytical procedures.

Characterization of waste - Preparation of test portions from the laboratory sample

HJ 711-2014 固体废物 酚类化合物的测定 气相色谱法

本标准规定了固体废物和固体废物浸出液中酚类化合物测定的气相色谱法。本标准适用于固体废物和固体废物浸出液中21种酚类化合物的测定,其他酚类化合物如果通过验证也可适用于本标准。当固体废物的取样量为10.0 g时,21种酚类化合物的方法检出限为0.02~0.33 mg/kg,测定下限为0.08~1.32 mg/kg,详见附录 A。当固体废物浸出液的取样量为100 ml时,21种酚类化合物的方法检出限为0.002~0.006 mg/L,测定下限为0.008~0.024 mg/L,详见附录A。

Solid waste.Determination of phenolic compounds.Gas chromatography

HJ 712-2014 固体废物 总磷的测定 偏钼酸铵分光光度法

本标准规定了测定固体废物中总磷的偏钼酸铵分光光度法。本标准适用于可粉碎的固态或半固态固体废物中总磷的测定。当取样量为0.5 g,定容体积为50 ml,使用30 mm比色皿时,本标准的方法检出限为3 mg/kg,测定下限为12 mg/kg。

Solid waste.Determination of total phosphorus.Ammonium metamolybdate spectrophotometric method

BS EN 16424:2014 废弃物的特性描述. 使用便携式X射线荧光光谱仪对元素成分进行的筛选方法

Characterization of waste. Screening methods for the element composition by portable X-ray fluorescence instruments

EN 16424:2014 废弃物的特性.用便携式X射线荧光设备进行元素组成的筛选方法

This European Standard is dedicated to field portable X-ray fluorescence (XRF) equipment (hand-held or portable bench top) and specifies a screening method for the determination of the elemental composition of waste materials for on-site verification. Portable XRF spectrometers are used for a rapid and exploratory analysis of paste-like or solid materials. The absence or presence of specific elements is displayed qualitatively with an indication of the concentration level.

Characterization of waste - Screening methods for the element composition by portable X-ray fluorescence instruments

ISO 11268-3:2014 土壤质量 污染物对蚯蚓的影响 第3部分:野外影响的测定指南

This part of ISO 11268 specifies techniques for determining the effects of substances on earthworms in the field and provides a basis for determining the effects of chemicals applied to or incorporated into soil, including soil injections or drilled pelleted formulations.

Soil quality - Effects of pollutants on earthworms - Part 3: Guidance on the determination of effects in field situations